(S)-N-(N-methyl-4,7-dihydrothieno<2,3-b>pyridine-5-carbonyl)phenylalaninol

Base Information

Chemical Name:(S)-N-(N-methyl-4,7-dihydrothieno<2,3-b>pyridine-5-carbonyl)phenylalaninol
CAS No.:121612-84-8
Molecular Formula:C₁₈H₂₀N₂O₂S
Molecular Weight:328.435
Hs Code.:

Synonyms:(S)-N-(N-methyl-4,7-dihydrothieno<2,3-b>pyridine-5-carbonyl)phenylalaninol

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Chemical Property of (S)-N-(N-methyl-4,7-dihydrothieno<2,3-b>pyridine-5-carbonyl)phenylalaninol

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Technology Process of (S)-N-(N-methyl-4,7-dihydrothieno<2,3-b>pyridine-5-carbonyl)phenylalaninol

There total 6 articles about (S)-N-(N-methyl-4,7-dihydrothieno<2,3-b>pyridine-5-carbonyl)phenylalaninol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 121612-79-1
5-((S)-1-Hydroxymethyl-2-phenyl-ethylcarbamoyl)-7-methyl-thieno[2,3-b]pyridin-7-ium; iodide

: 121612-84-8
(S)-N-(N-methyl-4,7-dihydrothieno<2,3-b>pyridine-5-carbonyl)phenylalaninol

Guidance literature:: With sodium dithionite; sodium carbonate; In methanol; water; for 0.333333h;

Reference yield:

: 117390-38-2
thieno<2,3-b>pyridine-5-carboxylic acid

: 121612-84-8
(S)-N-(N-methyl-4,7-dihydrothieno<2,3-b>pyridine-5-carbonyl)phenylalaninol

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 12 h / Heating

2: 73 percent / Et₃N / CH₂Cl₂ / 1) -20 deg C, 1 h, 2) room temperature, 24 h

3: acetonitrile / 8 h / Heating

4: 94 percent / Na₂CO₃*10H₂O, Na₂S₂O₄ / methanol; H₂O / 0.33 h

With thionyl chloride; sodium dithionite; sodium carbonate; triethylamine; In methanol; dichloromethane; water; acetonitrile;

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 121612-84-8
(S)-N-(N-methyl-4,7-dihydrothieno<2,3-b>pyridine-5-carbonyl)phenylalaninol

Guidance literature:: Multi-step reaction with 4 steps

1: LiAlH₄

2: 73 percent / Et₃N / CH₂Cl₂ / 1) -20 deg C, 1 h, 2) room temperature, 24 h

3: acetonitrile / 8 h / Heating

4: 94 percent / Na₂CO₃*10H₂O, Na₂S₂O₄ / methanol; H₂O / 0.33 h

With lithium aluminium tetrahydride; sodium dithionite; sodium carbonate; triethylamine; In methanol; dichloromethane; water; acetonitrile;