(6,6-dimethyl-4-phenyl-2-oxo-5,6-dihydro-4H-[1,2]oxazin-3-yl)methyl formate

Base Information

Chemical Name:(6,6-dimethyl-4-phenyl-2-oxo-5,6-dihydro-4H-[1,2]oxazin-3-yl)methyl formate
CAS No.:1313227-90-5
Molecular Formula:C₁₄H₁₇NO₄
Molecular Weight:263.293
Hs Code.:

Synonyms:(6,6-dimethyl-4-phenyl-2-oxo-5,6-dihydro-4H-[1,2]oxazin-3-yl)methyl formate

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Chemical Property of (6,6-dimethyl-4-phenyl-2-oxo-5,6-dihydro-4H-[1,2]oxazin-3-yl)methyl formate

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Technology Process of (6,6-dimethyl-4-phenyl-2-oxo-5,6-dihydro-4H-[1,2]oxazin-3-yl)methyl formate

There total 3 articles about (6,6-dimethyl-4-phenyl-2-oxo-5,6-dihydro-4H-[1,2]oxazin-3-yl)methyl formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 929878-91-1
3-(bromomethyl)-6,6-dimethyl-4-phenyl-5,6-dihydro-4H-[1,2]oxazine 2-oxide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1313227-90-5
(6,6-dimethyl-4-phenyl-2-oxo-5,6-dihydro-4H-[1,2]oxazin-3-yl)methyl formate

Guidance literature:: With silver fluoride; at -40 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2011.04.078

Reference yield:

: 638133-16-1
6,6-dimethyl-3-methylene-4-phenyl-2-(trimethylsilyloxy)-2,3,5,6-tetrahydro-4H-[1,2]oxazine

: 1313227-90-5
(6,6-dimethyl-4-phenyl-2-oxo-5,6-dihydro-4H-[1,2]oxazin-3-yl)methyl formate

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / dichloromethane / -78 - 20 °C / Inert atmosphere

2: silver fluoride / 1 h / -40 °C / Inert atmosphere

With N-Bromosuccinimide; silver fluoride; In dichloromethane;
DOI:10.1016/j.tet.2011.04.078

Reference yield:

: 638133-04-7
6,6-dimethyl-5,6-dihydro-3-methyl-4-phenyl-1,2-oxazine N-oxide

: 1313227-90-5
(6,6-dimethyl-4-phenyl-2-oxo-5,6-dihydro-4H-[1,2]oxazin-3-yl)methyl formate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 3 h / -78 °C / Inert atmosphere

2: N-Bromosuccinimide / dichloromethane / -78 - 20 °C / Inert atmosphere

3: silver fluoride / 1 h / -40 °C / Inert atmosphere

With N-Bromosuccinimide; silver fluoride; triethylamine; In dichloromethane;
DOI:10.1016/j.tet.2011.04.078