benzyl (1R)-2,2-dimethyl-1-((4-(3-oxo-4-morpholinyl)-1-piperidinyl)carbonyl)propylcarbamate

Base Information

Chemical Name:benzyl (1R)-2,2-dimethyl-1-((4-(3-oxo-4-morpholinyl)-1-piperidinyl)carbonyl)propylcarbamate
CAS No.:856418-58-1
Molecular Formula:C₂₃H₃₃N₃O₅
Molecular Weight:431.532
Hs Code.:

Synonyms:benzyl (1R)-2,2-dimethyl-1-((4-(3-oxo-4-morpholinyl)-1-piperidinyl)carbonyl)propylcarbamate

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Chemical Property of benzyl (1R)-2,2-dimethyl-1-((4-(3-oxo-4-morpholinyl)-1-piperidinyl)carbonyl)propylcarbamate

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Technology Process of benzyl (1R)-2,2-dimethyl-1-((4-(3-oxo-4-morpholinyl)-1-piperidinyl)carbonyl)propylcarbamate

There total 1 articles about benzyl (1R)-2,2-dimethyl-1-((4-(3-oxo-4-morpholinyl)-1-piperidinyl)carbonyl)propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 856418-57-0
tert-butyl 4-(3-oxo-4-morpholinyl)-1-piperidinecarboxylate

: 70874-05-4
Z-D-Tle

: 856418-58-1
benzyl (1R)-2,2-dimethyl-1-((4-(3-oxo-4-morpholinyl)-1-piperidinyl)carbonyl)propylcarbamate

Guidance literature:: tert-butyl 4-(3-oxo-4-morpholinyl)-1-piperidinecarboxylate; With trifluoroacetic acid; In dichloromethane; ethyl acetate; at 20 ℃; for 2h;

Z-D-Tle; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In acetonitrile; at 20 ℃; for 15h;

Reference yield: 93.0%

: 856418-58-1
benzyl (1R)-2,2-dimethyl-1-((4-(3-oxo-4-morpholinyl)-1-piperidinyl)carbonyl)propylcarbamate

: 104-12-1
p-chlorphenylisocyanate

: N-(4-chlorophenyl)-N'-((1R)-2,2-dimethyl-1-((4-(3-oxo-4-morpholinyl)-1-piperidinyl)carbonyl)propyl)urea

Guidance literature:: benzyl (1R)-2,2-dimethyl-1-((4-(3-oxo-4-morpholinyl)-1-piperidinyl)carbonyl)propylcarbamate; With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; for 2h;

p-chlorphenylisocyanate; In acetonitrile; at 20 ℃; for 1h;