C₂₅H₃₆O₇

Base Information

Chemical Name:C₂₅H₃₆O₇
CAS No.:391278-05-0
Molecular Formula:C₂₅H₃₆O₇
Molecular Weight:448.557
Hs Code.:

C<sub>25</sub>H<sub>36</sub>O<sub>7</sub>

Synonyms:C₂₅H₃₆O₇

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Chemical Property of C₂₅H₃₆O₇

Chemical Property:

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Technology Process of C₂₅H₃₆O₇

There total 21 articles about C₂₅H₃₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 391278-04-9
C₂₅H₃₄O₇

: 391278-05-0
C₂₅H₃₆O₇

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.5h;
DOI:10.1016/j.tet.2004.07.094

Reference yield:

: 2244-16-8,6485-40-1
(S)-p-mentha-6,8-dien-2-one

: 391278-05-0
C₂₅H₃₆O₇

Guidance literature:: Multi-step reaction with 14 steps

1.1: 92 percent / EtAlCl₂ / toluene; hexane / 28 h / 20 °C

2.1: 89 percent / p-TsOH / benzene / 12 h / Heating

3.1: N-methylmorpholine-N-oxide; OsO₄ / acetone; H₂O / 216 h / 20 °C

3.2: 74 percent / NaIO₄ / acetone; H₂O / 1 h / 20 °C

4.1: 93 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 72 h / 20 °C

5.1: 92 percent / p-TsOH / CH₂Cl₂ / 24 h / 20 °C

6.1: K₂CO₃ / methanol / 4 h / 20 °C

6.2: 90 percent / PCC / CH₂Cl₂ / 3 h / 20 °C

7.1: 88 percent / Et₃N / CH₂Cl₂ / 0.5 h / -78 °C

8.1: 73 percent / Na₂(EDTA); oxone; NaHCO₃ / H₂O; acetone; acetonitrile / 4 h / 20 °C

9.1: 79 percent / Al(OiPr)3 / toluene / 1 h / 20 °C

10.1: Me₃SiCl; Et₃N; DMAP / CH₂Cl₂ / 0.33 h / 20 °C

10.2: tetrahydrofuran / 0.17 h / -78 °C

10.3: 90 percent / HCl / tetrahydrofuran; H₂O / 0.5 h / 20 °C

11.1: NaH / tetrahydrofuran / 0 - 20 °C

11.2: 86 percent / tetrahydrofuran / 12 h / Heating

12.1: OsO₄; N-methylmorpholine-N-oxide / acetone; H₂O / 96 h / 20 °C

12.2: 78 percent / NaIO₄ / acetone; H₂O / 48 h / 20 °C

13.1: 70 percent / H₂ / Pd/C / ethyl acetate

14.1: 100 percent / NaBH₄ / methanol / 0.5 h / 0 °C

With dmap; Oxone; sodium tetrahydroborate; osmium(VIII) oxide; chloro-trimethyl-silane; hydrogen; ethylaluminum dichloride; edetate disodium; aluminum isopropoxide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; benzene; 1.1: Diels-Alder reaction / 4.1: Baeyer-Villiger oxidation;
DOI:10.1016/j.tet.2004.07.094

Reference yield:

: 391277-97-7
C₁₆H₂₆O₆

: 391278-05-0
C₂₅H₃₆O₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: 92 percent / p-TsOH / CH₂Cl₂ / 24 h / 20 °C

2.1: K₂CO₃ / methanol / 4 h / 20 °C

2.2: 90 percent / PCC / CH₂Cl₂ / 3 h / 20 °C

3.1: 88 percent / Et₃N / CH₂Cl₂ / 0.5 h / -78 °C

4.1: 73 percent / Na₂(EDTA); oxone; NaHCO₃ / H₂O; acetone; acetonitrile / 4 h / 20 °C

5.1: 79 percent / Al(OiPr)3 / toluene / 1 h / 20 °C

6.1: Me₃SiCl; Et₃N; DMAP / CH₂Cl₂ / 0.33 h / 20 °C

6.2: tetrahydrofuran / 0.17 h / -78 °C

6.3: 90 percent / HCl / tetrahydrofuran; H₂O / 0.5 h / 20 °C

7.1: NaH / tetrahydrofuran / 0 - 20 °C

7.2: 86 percent / tetrahydrofuran / 12 h / Heating

8.1: OsO₄; N-methylmorpholine-N-oxide / acetone; H₂O / 96 h / 20 °C

8.2: 78 percent / NaIO₄ / acetone; H₂O / 48 h / 20 °C

9.1: 70 percent / H₂ / Pd/C / ethyl acetate

10.1: 100 percent / NaBH₄ / methanol / 0.5 h / 0 °C

With dmap; Oxone; sodium tetrahydroborate; osmium(VIII) oxide; chloro-trimethyl-silane; hydrogen; edetate disodium; aluminum isopropoxide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile;
DOI:10.1016/j.tet.2004.07.094