methyl 4-[(3S,4S,5R)-1-(toluene-4-sulphonyl)-3-triisopropylsilanyloxy-5-trityloxymethylpiperidin-4-yl]benzoate

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Chemical Name:methyl 4-[(3S,4S,5R)-1-(toluene-4-sulphonyl)-3-triisopropylsilanyloxy-5-trityloxymethylpiperidin-4-yl]benzoate
CAS No.:912347-28-5
Molecular Formula:C₄₉H₅₉NO₆SSi
Molecular Weight:818.162
Hs Code.:
Mol file:912347-28-5.mol

Synonyms:methyl 4-[(3S,4S,5R)-1-(toluene-4-sulphonyl)-3-triisopropylsilanyloxy-5-trityloxymethylpiperidin-4-yl]benzoate

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Chemical Property of methyl 4-[(3S,4S,5R)-1-(toluene-4-sulphonyl)-3-triisopropylsilanyloxy-5-trityloxymethylpiperidin-4-yl]benzoate Edit

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Technology Process of methyl 4-[(3S,4S,5R)-1-(toluene-4-sulphonyl)-3-triisopropylsilanyloxy-5-trityloxymethylpiperidin-4-yl]benzoate

There total 2 articles about methyl 4-[(3S,4S,5R)-1-(toluene-4-sulphonyl)-3-triisopropylsilanyloxy-5-trityloxymethylpiperidin-4-yl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 912347-29-6
methyl 4-[(3S,4S,5R)-3-hydroxy-1-(toluene-4-sulphonyl)-5-trityloxymethylpiperidin-4-yl]benzoate

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 912347-28-5
methyl 4-[(3S,4S,5R)-1-(toluene-4-sulphonyl)-3-triisopropylsilanyloxy-5-trityloxymethylpiperidin-4-yl]benzoate

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 3.16667h;

Reference yield:

: 912347-30-9
methyl 4-[(3S,4S,5R)-3-hydroxy-5-hydroxymethyl-1-(toluene-4-sulphonyl)-piperidin-4-yl]-benzoate

: 76-83-5
trityl chloride

: 912347-28-5
methyl 4-[(3S,4S,5R)-1-(toluene-4-sulphonyl)-3-triisopropylsilanyloxy-5-trityloxymethylpiperidin-4-yl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / pyridine / 12 h / 70 °C

2: 2,6-dimethylpyridine / dichloromethane / 3.17 h / 0 °C

With 2,6-dimethylpyridine; dmap; In pyridine; dichloromethane;