(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate

Base Information

Chemical Name:(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate
CAS No.:835905-83-4
Molecular Formula:C₁₅H₁₈O₇
Molecular Weight:310.304
Hs Code.:

Synonyms:(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate

Suppliers and Price of (2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate

There total 3 articles about (2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 170428-69-0
C₁₂H₁₇NO₇

: 621-82-9
Cinnamic acid

: 835905-83-4
(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate

: 41682-52-4
(2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate

Guidance literature:: In toluene; at 70 ℃; for 16h; optical yield given as %de; diastereoselective reaction;
DOI:10.1016/j.tetlet.2011.08.104

Reference yield:

: 170428-43-0
C₂₀H₂₅NO₁₁

: 835905-83-4
(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate

: 41682-52-4
(2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate

Guidance literature:: Multi-step reaction with 3 steps

1: mercury dibromide / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / Reflux

2: sodium methylate / methanol / 0.25 h / 20 °C / Reflux

3: toluene / 16 h / 70 °C

With sodium methylate; mercury dibromide; In methanol; 5,5-dimethyl-1,3-cyclohexadiene; toluene;
DOI:10.1016/j.tetlet.2011.08.104

Reference yield:

: 170428-45-2
C₂₀H₂₅NO₁₁

: 835905-83-4
(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate

: 41682-52-4
(2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl cinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 0.25 h / 20 °C / Reflux

2: toluene / 16 h / 70 °C

With sodium methylate; In methanol; toluene;
DOI:10.1016/j.tetlet.2011.08.104