C₂₅H₂₁N₃

Base Information

Chemical Name:C₂₅H₂₁N₃
CAS No.:1397718-31-8
Molecular Formula:C₂₅H₂₁N₃
Molecular Weight:363.462
Hs Code.:

C<sub>25</sub>H<sub>21</sub>N<sub>3</sub>

Synonyms:C₂₅H₂₁N₃

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Chemical Property of C₂₅H₂₁N₃

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Technology Process of C₂₅H₂₁N₃

There total 2 articles about C₂₅H₂₁N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1359973-18-4
3-cyclopentyl-2-iodo-3H-imidazo[4,5-b]pyridine

: 58650-11-6
3-Biphenylylacetylene

: 1397718-31-8
C₂₅H₂₁N₃

Guidance literature:: 3-cyclopentyl-2-iodo-3H-imidazo[4,5-b]pyridine; 3-Biphenylylacetylene; With tetrabutylammonium acetate; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 0.15h; Inert atmosphere;

With (bis(tricyclohexyl)phosphine)palladium(II) dichloride; In 1-methyl-pyrrolidin-2-one; at 110 ℃; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.tetlet.2012.07.028

Reference yield:

: 1359973-16-2
3-cyclopentyl-3H-imidazo[4,5-b]pyridine

: 1397718-31-8
C₂₅H₂₁N₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium; carbon tetrabromide / -78 °C

2.1: tetrabutylammonium acetate / 1-methyl-pyrrolidin-2-one / 0.15 h / 20 °C / Inert atmosphere

2.2: 110 °C / Inert atmosphere; Microwave irradiation

With carbon tetrabromide; tert.-butyl lithium; tetrabutylammonium acetate; In 1-methyl-pyrrolidin-2-one; 2.1: |Sonogashira Cross-Coupling / 2.2: |Sonogashira Cross-Coupling;
DOI:10.1016/j.tetlet.2012.07.028