(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2-(3-methoxyphenyl)-3-phenylpropanoate

Base Information

Chemical Name:(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2-(3-methoxyphenyl)-3-phenylpropanoate
CAS No.:1431563-80-2
Molecular Formula:C₂₃H₃₂O₄Si
Molecular Weight:400.59
Hs Code.:

Synonyms:(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2-(3-methoxyphenyl)-3-phenylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2-(3-methoxyphenyl)-3-phenylpropanoate

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Technology Process of (2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2-(3-methoxyphenyl)-3-phenylpropanoate

There total 1 articles about (2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2-(3-methoxyphenyl)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 53172-91-1
(benzyloxy)(tert-butyl)dimethylsilane

: 384365-49-5
methyl 2-diazo-2-(3-methoxyphenyl)acetate

: 1431563-80-2
(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2-(3-methoxyphenyl)-3-phenylpropanoate

Guidance literature:: With dirhodium(II) tetrakis[N-phthaloyl-(S)-tert-leucinate]; at 50 ℃; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja401731d

Reference yield: 89.0%

: 1431563-80-2
(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2-(3-methoxyphenyl)-3-phenylpropanoate

: 1431563-95-9
(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2,3-diphenylpropanoate

Guidance literature:: With hydrogenchloride; In ethanol; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja401731d

Reference yield:

: 1431563-80-2
(2S,3S)-methyl 3-((tert-butyldimethylsilyl)oxy)-2-(3-methoxyphenyl)-3-phenylpropanoate

: 1431564-05-4
(2S,3S)-methyl 5-methoxy-2-phenyl-2,3-dihydrobenzofuran-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol / 0 - 20 °C / Inert atmosphere

2: [bis(acetoxy)iodo]benzene; lithium carbonate; palladium diacetate / Hexafluorobenzene / 24 h / 100 °C / Inert atmosphere

With hydrogenchloride; [bis(acetoxy)iodo]benzene; palladium diacetate; lithium carbonate; In Hexafluorobenzene; ethanol;
DOI:10.1021/ja401731d