(Z)-1-fluoro-2-phenylethenyl 2-(trimethylsilyl)ethyl butyldicarbonimidoate

Base Information

Chemical Name:(Z)-1-fluoro-2-phenylethenyl 2-(trimethylsilyl)ethyl butyldicarbonimidoate
CAS No.:1354974-34-7
Molecular Formula:C₁₉H₂₈FNO₄Si
Molecular Weight:381.52
Hs Code.:

Synonyms:(Z)-1-fluoro-2-phenylethenyl 2-(trimethylsilyl)ethyl butyldicarbonimidoate

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Chemical Property of (Z)-1-fluoro-2-phenylethenyl 2-(trimethylsilyl)ethyl butyldicarbonimidoate

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Technology Process of (Z)-1-fluoro-2-phenylethenyl 2-(trimethylsilyl)ethyl butyldicarbonimidoate

There total 2 articles about (Z)-1-fluoro-2-phenylethenyl 2-(trimethylsilyl)ethyl butyldicarbonimidoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1354974-24-5
2,2-dibromo-2-fluoro-1-phenylethyl 2-(trimethylsilyl)ethyl butyldicarbonimidoate

: 1354974-34-7
(Z)-1-fluoro-2-phenylethenyl 2-(trimethylsilyl)ethyl butyldicarbonimidoate

Guidance literature:: With chromium dichloride; manganese; In tetrahydrofuran; at 20 ℃; for 20h; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.jfluchem.2011.07.022

Reference yield:

: 2-trimethylsilylethyl-N-n-butylcarbamate

: 1354974-34-7
(Z)-1-fluoro-2-phenylethenyl 2-(trimethylsilyl)ethyl butyldicarbonimidoate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 21 h / -30 - 20 °C / Inert atmosphere

2: triethylamine / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

3: chromium dichloride; manganese / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

With pyridine; chromium dichloride; manganese; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.jfluchem.2011.07.022

Reference yield: 95.0%

: 1354974-34-7
(Z)-1-fluoro-2-phenylethenyl 2-(trimethylsilyl)ethyl butyldicarbonimidoate

: 1354974-59-6
(Z)-1-fluoro-2-phenylethenyl butyldicarbonimidoate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1016/j.jfluchem.2011.07.022