phenyl 4-O-acetyl-2-O-allyl-3-O-p-methoxybenzyl-1-thio-β-L-fucopyranoside

Base Information

Chemical Name:phenyl 4-O-acetyl-2-O-allyl-3-O-p-methoxybenzyl-1-thio-β-L-fucopyranoside
CAS No.:1334671-96-3
Molecular Formula:C₂₅H₃₀O₆S
Molecular Weight:458.576
Hs Code.:

Synonyms:phenyl 4-O-acetyl-2-O-allyl-3-O-p-methoxybenzyl-1-thio-β-L-fucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 4-O-acetyl-2-O-allyl-3-O-p-methoxybenzyl-1-thio-β-L-fucopyranoside

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Technology Process of phenyl 4-O-acetyl-2-O-allyl-3-O-p-methoxybenzyl-1-thio-β-L-fucopyranoside

There total 4 articles about phenyl 4-O-acetyl-2-O-allyl-3-O-p-methoxybenzyl-1-thio-β-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₈O₅S

: 108-24-7
acetic anhydride

: 1334671-96-3
phenyl 4-O-acetyl-2-O-allyl-3-O-p-methoxybenzyl-1-thio-β-L-fucopyranoside

Guidance literature:: With pyridine; for 7h;
DOI:10.1016/j.carres.2011.06.027

Reference yield:

: 196397-59-8
phenyl 3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

: 1334671-96-3
phenyl 4-O-acetyl-2-O-allyl-3-O-p-methoxybenzyl-1-thio-β-L-fucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

1.2: 1 h / 0 - 20 °C

2.1: acetic acid / water / 2 h / 60 °C

3.1: di(n-butyl)tin oxide / benzene / 16 h / Reflux

3.2: 5 h / Reflux

4.1: pyridine / 7 h

With pyridine; sodium hydride; di(n-butyl)tin oxide; acetic acid; In water; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.carres.2011.06.027

Reference yield:

: 1334671-92-9
phenyl 2-O-allyl-3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

: 1334671-96-3
phenyl 4-O-acetyl-2-O-allyl-3-O-p-methoxybenzyl-1-thio-β-L-fucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / water / 2 h / 60 °C

2.1: di(n-butyl)tin oxide / benzene / 16 h / Reflux

2.2: 5 h / Reflux

3.1: pyridine / 7 h

With pyridine; di(n-butyl)tin oxide; acetic acid; In water; benzene;
DOI:10.1016/j.carres.2011.06.027