(1'RS,2'E,3RS,R_SS_S)-<1'-methyl-3'-(phenylsulfinyl)prop-2'-enyl>butan-4-olide

Base Information

Chemical Name:(1'RS,2'E,3RS,R_SS_S)-<1'-methyl-3'-(phenylsulfinyl)prop-2'-enyl>butan-4-olide
CAS No.:114678-68-1
Molecular Formula:C₁₄H₁₆O₃S
Molecular Weight:264.345
Hs Code.:

(1'RS,2'E,3RS,R<sub>S</sub>S<sub>S</sub>)-<1'-methyl-3'-(phenylsulfinyl)prop-2'-enyl>butan-4-olide

Synonyms:(1'RS,2'E,3RS,R_SS_S)-<1'-methyl-3'-(phenylsulfinyl)prop-2'-enyl>butan-4-olide

Suppliers and Price of (1'RS,2'E,3RS,R_SS_S)-<1'-methyl-3'-(phenylsulfinyl)prop-2'-enyl>butan-4-olide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1'RS,2'E,3RS,R_SS_S)-<1'-methyl-3'-(phenylsulfinyl)prop-2'-enyl>butan-4-olide

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Technology Process of (1'RS,2'E,3RS,R_SS_S)-<1'-methyl-3'-(phenylsulfinyl)prop-2'-enyl>butan-4-olide

There total 2 articles about (1'RS,2'E,3RS,R_SS_S)-<1'-methyl-3'-(phenylsulfinyl)prop-2'-enyl>butan-4-olide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 702-04-5
crotyl phenyl sulfide

: 114678-68-1
(1'RS,2'E,3RS,R_SS_S)-<1'-methyl-3'-(phenylsulfinyl)prop-2'-enyl>butan-4-olide

Guidance literature:: Multi-step reaction with 2 steps

1: m-chloroperbenzoic acid / CH₂Cl₂ / -70 °C

2: 1.) lithium diisopropylamide / 1.) THF, -70 deg C, 5 min, 2.) THF, -70 deg C

With 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In dichloromethane;
DOI:10.1021/ja00224a029

Reference yield:

: 497-23-4
2-buten-4-olide

: 42185-87-5,128441-92-9,128441-93-0
1-(phenylsulfinyl)but-2-ene

: 114718-14-8
(1'RS,2'E,3SR,S_SR_S)-<1'-methyl-3'-(phenylsulfinyl)prop-2'-enyl>butan-4-olide

: 114678-68-1
(1'RS,2'E,3RS,R_SS_S)-<1'-methyl-3'-(phenylsulfinyl)prop-2'-enyl>butan-4-olide

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, -70 deg C, 5 min, 2.) THF, -70 deg C;
DOI:10.1021/ja00224a029