N₆-acetyl-3-butyl-4-diphenylphosphinosidnoimine palladiumdichloride

Base Information

• Chemical Name: N₆-acetyl-3-butyl-4-diphenylphosphinosidnoimine palladiumdichloride
• CAS No.: 1187641-89-9
• Molecular Formula: C₂₀H₂₂Cl₂N₃O₂PPd
• Molecular Weight: 544.713
• Mol file: 1187641-89-9.mol

Synonyms:N₆-acetyl-3-butyl-4-diphenylphosphinosidnoimine palladiumdichloride

Chemical Property of N₆-acetyl-3-butyl-4-diphenylphosphinosidnoimine palladiumdichloride

Chemical Property:

Purity/Quality:

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Technology Process of N₆-acetyl-3-butyl-4-diphenylphosphinosidnoimine palladiumdichloride

There total 1 articles about N₆-acetyl-3-butyl-4-diphenylphosphinosidnoimine palladiumdichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

dichloro bis(acetonitrile) palladium(II) (21264-30-2,90243-59-7,14592-56-4) + N6-acetyl-3-butyl-4-diphenylphosphinosidnoimine (1187641-83-3) → N6-acetyl-3-butyl-4-diphenylphosphinosidnoimine palladiumdichloride (1187641-89-9)

Guidance literature:

With n-BuLi; In acetonitrile; under Ar; to sidnonimine in MeCN Pd complex added; stirred for 30 min atroom temp.; solvent removed under reduced pressure; residue crystd. from MeCN/ether;elem. anal.;

DOI:10.1016/j.poly.2009.04.038

upstream raw materials:

dichloro bis(acetonitrile) palladium(II)

N₆-acetyl-3-butyl-4-diphenylphosphinosidnoimine