(1S,5S,1'S)-6,8-bis(1'-phenylethyl)-7,9-dioxo-1-allyl-3-methylene-6,8-diazabicyclo[3.2.2]nonane

Base Information

Chemical Name:(1S,5S,1'S)-6,8-bis(1'-phenylethyl)-7,9-dioxo-1-allyl-3-methylene-6,8-diazabicyclo[3.2.2]nonane
CAS No.:530125-17-8
Molecular Formula:C₂₇H₃₀N₂O₂
Molecular Weight:414.547
Hs Code.:

Synonyms:(1S,5S,1'S)-6,8-bis(1'-phenylethyl)-7,9-dioxo-1-allyl-3-methylene-6,8-diazabicyclo[3.2.2]nonane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,5S,1'S)-6,8-bis(1'-phenylethyl)-7,9-dioxo-1-allyl-3-methylene-6,8-diazabicyclo[3.2.2]nonane

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Technology Process of (1S,5S,1'S)-6,8-bis(1'-phenylethyl)-7,9-dioxo-1-allyl-3-methylene-6,8-diazabicyclo[3.2.2]nonane

There total 2 articles about (1S,5S,1'S)-6,8-bis(1'-phenylethyl)-7,9-dioxo-1-allyl-3-methylene-6,8-diazabicyclo[3.2.2]nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 106-95-6
allyl bromide

: 530125-07-6
(1S,5S,1'S)-6,8-bis(1'-phenylethyl)-7,9-dioxo-3-methylene-6,8-diazabicyclo[3.2.2]nonane

: (1S,5S)-3-Methylene-6-(1-methyl-1-phenyl-but-3-enyl)-8-((S)-1-phenyl-ethyl)-6,8-diaza-bicyclo[3.2.2]nonane-7,9-dione

: 530125-17-8
(1S,5S,1'S)-6,8-bis(1'-phenylethyl)-7,9-dioxo-1-allyl-3-methylene-6,8-diazabicyclo[3.2.2]nonane

Guidance literature:: With methyllithium; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1016/S0957-4166(02)00834-0

Reference yield:

: 158547-56-9
1,4-N,N-[(S)-1-phenylethyl]-piperazine-2,5-dione

: 530125-17-8
(1S,5S,1'S)-6,8-bis(1'-phenylethyl)-7,9-dioxo-1-allyl-3-methylene-6,8-diazabicyclo[3.2.2]nonane

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / LHMDS / tetrahydrofuran / -78 - 20 °C

2: 76 percent / CH₃Li / tetrahydrofuran / -78 - 20 °C

With methyllithium; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1016/S0957-4166(02)00834-0