Technology Process of 2-aminomethyl-1-phenylpyrrole
There total 4 articles about 2-aminomethyl-1-phenylpyrrole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol;
for 6h;
under 3040 Torr;
Ambient temperature;
DOI:10.1055/s-1994-25429
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 90 percent / diethyl ether / 8 h / 20 - 24 °C
2: 80 percent / NaN3, 18-crown-6 / dioxane / 12 h / Heating
3: 80 percent / H2 / 10 percent Pd-C / methanol / 6 h / 3040 Torr / Ambient temperature
With
sodium azide; 18-crown-6 ether; hydrogen;
palladium on activated charcoal;
In
1,4-dioxane; methanol; diethyl ether;
DOI:10.1055/s-1994-25429
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 80 percent / NaN3, 18-crown-6 / dioxane / 12 h / Heating
2: 80 percent / H2 / 10 percent Pd-C / methanol / 6 h / 3040 Torr / Ambient temperature
With
sodium azide; 18-crown-6 ether; hydrogen;
palladium on activated charcoal;
In
1,4-dioxane; methanol;
DOI:10.1055/s-1994-25429
