3-(4-(3-(3,4-dimethoxyphenyl)pyrazolo[1,5-a]pyrimidin-5-yl)-2-methoxyphenoxy)propylamine

Base Information

Chemical Name:3-(4-(3-(3,4-dimethoxyphenyl)pyrazolo[1,5-a]pyrimidin-5-yl)-2-methoxyphenoxy)propylamine
CAS No.:1084951-41-6
Molecular Formula:C₂₄H₂₆N₄O₄
Molecular Weight:434.495
Hs Code.:

Synonyms:3-(4-(3-(3,4-dimethoxyphenyl)pyrazolo[1,5-a]pyrimidin-5-yl)-2-methoxyphenoxy)propylamine

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Chemical Property of 3-(4-(3-(3,4-dimethoxyphenyl)pyrazolo[1,5-a]pyrimidin-5-yl)-2-methoxyphenoxy)propylamine

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Technology Process of 3-(4-(3-(3,4-dimethoxyphenyl)pyrazolo[1,5-a]pyrimidin-5-yl)-2-methoxyphenoxy)propylamine

There total 5 articles about 3-(4-(3-(3,4-dimethoxyphenyl)pyrazolo[1,5-a]pyrimidin-5-yl)-2-methoxyphenoxy)propylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1084951-40-5
(3-(4-(3-(3,4-dimethoxyphenyl)pyrazolo[1,5-a]pyrimidin-5-yl)-2-methoxyphenoxy)propyl)carbamic acid tert-butyl ester

: 1084951-41-6
3-(4-(3-(3,4-dimethoxyphenyl)pyrazolo[1,5-a]pyrimidin-5-yl)-2-methoxyphenoxy)propylamine

Guidance literature:: (3-(4-(3-(3,4-dimethoxyphenyl)pyrazolo[1,5-a]pyrimidin-5-yl)-2-methoxyphenoxy)propyl)carbamic acid tert-butyl ester; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 3h;

With sodium hydrogencarbonate; In 1,4-dioxane; water;

Reference yield:

: 1084953-04-7
3-(3,4-dimethoxy-phenyl)-4H-pyrazolo[1,5-a]pyrimidin-5-one

: 1084951-41-6
3-(4-(3-(3,4-dimethoxyphenyl)pyrazolo[1,5-a]pyrimidin-5-yl)-2-methoxyphenoxy)propylamine

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / 48 h / 120 °C

2: potassium carbonate / bis-triphenylphosphine-palladium(II) chloride / water; N,N-dimethyl-formamide / 1.5 h / 120 °C

3: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

With hydrogenchloride; potassium carbonate; trichlorophosphate; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; water; N,N-dimethyl-formamide;

Reference yield:

: 269410-22-2
4-hydroxy-3-methoxyphenylboronic acid pinacol ester

: 1084951-41-6
3-(4-(3-(3,4-dimethoxyphenyl)pyrazolo[1,5-a]pyrimidin-5-yl)-2-methoxyphenoxy)propylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 18 h / 0 - 20 °C

2.1: potassium carbonate / bis-triphenylphosphine-palladium(II) chloride / water; N,N-dimethyl-formamide / 1.5 h / 120 °C

3.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

With hydrogenchloride; sodium hydride; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; water; N,N-dimethyl-formamide;