meso-3,5-bis<<(1,1-dimethylethoxy)carbonyl>amino>-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine

Base Information

Chemical Name:meso-3,5-bis<<(1,1-dimethylethoxy)carbonyl>amino>-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine
CAS No.:152663-90-6
Molecular Formula:C₂₇H₃₅N₃O₄
Molecular Weight:465.593
Hs Code.:

meso-3,5-bis<<(1,1-dimethylethoxy)carbonyl>amino>-1,2,3,5,6,7-hexahydro-8-phenyldicyclopenta<b,e>pyridine

Synonyms:meso-3,5-bis<<(1,1-dimethylethoxy)carbonyl>amino>-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine

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Chemical Property of meso-3,5-bis<<(1,1-dimethylethoxy)carbonyl>amino>-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine

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Technology Process of meso-3,5-bis<<(1,1-dimethylethoxy)carbonyl>amino>-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine

There total 2 articles about meso-3,5-bis<<(1,1-dimethylethoxy)carbonyl>amino>-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 909204-77-9
3,5-diamino-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine

: 152663-90-6
meso-3,5-bis<<(1,1-dimethylethoxy)carbonyl>amino>-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine

: d,l-3,5-bis<<(1,1-dimethylethoxy)carbonyl>amino>-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine

Guidance literature:: In chloroform; for 0.75h;
DOI:10.1021/ja00075a021

Reference yield:

: 3,5-bis(hydroxyimino)-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine

: 152663-90-6
meso-3,5-bis<<(1,1-dimethylethoxy)carbonyl>amino>-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NaBH₄, TiCl₄ / 1,2-dimethoxy-ethane / 24 h / Ambient temperature

2: 50 percent / CHCl₃ / 0.75 h

With sodium tetrahydroborate; titanium tetrachloride; In 1,2-dimethoxyethane; chloroform;
DOI:10.1021/ja00075a021

Reference yield:

: 152663-90-6
meso-3,5-bis<<(1,1-dimethylethoxy)carbonyl>amino>-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine

: 152663-97-3
meso-3,5-bis<<<<2-<<(1,1-dimethylethoxy)carbonyl>amino>ethyl>amino>thioxomethyl>amino>-1,2,3,5,6,7-hexahydro-8-phenyldicyclopentapyridine

Guidance literature:: Multi-step reaction with 2 steps

1: TFA, H₂O / 4 h

2: 100 percent / ethanol / 20 h

With water; trifluoroacetic acid; In ethanol;
DOI:10.1021/ja00075a021