phenyl 6-O-(tert-butyldiphenylsilyl)-3,4-O-isopropylidene-1-thio-α-D-talopyranoside

Base Information

Chemical Name:phenyl 6-O-(tert-butyldiphenylsilyl)-3,4-O-isopropylidene-1-thio-α-D-talopyranoside
CAS No.:1207163-07-2
Molecular Formula:C₃₁H₃₈O₅SSi
Molecular Weight:550.791
Hs Code.:

Synonyms:phenyl 6-O-(tert-butyldiphenylsilyl)-3,4-O-isopropylidene-1-thio-α-D-talopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 6-O-(tert-butyldiphenylsilyl)-3,4-O-isopropylidene-1-thio-α-D-talopyranoside

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Technology Process of phenyl 6-O-(tert-butyldiphenylsilyl)-3,4-O-isopropylidene-1-thio-α-D-talopyranoside

There total 1 articles about phenyl 6-O-(tert-butyldiphenylsilyl)-3,4-O-isopropylidene-1-thio-α-D-talopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₃₆O₅SSi

: 1207163-07-2
phenyl 6-O-(tert-butyldiphenylsilyl)-3,4-O-isopropylidene-1-thio-α-D-talopyranoside

: phenyl 6-O-(tert-butyldiphenylsilyl)-3,4-O-isopropylidene-1-thio-β-D-talopyranoside

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.333333h; optical yield given as %de; Inert atmosphere;
DOI:10.1039/b916580k

Reference yield: 89.0%

: 1207163-07-2
phenyl 6-O-(tert-butyldiphenylsilyl)-3,4-O-isopropylidene-1-thio-α-D-talopyranoside

: 108-24-7
acetic anhydride

: 1207163-05-0
phenyl 2-O-acetyl-6-O-(tert-butyldiphenylsilyl)-3,4-O-isopropylidene-1-thio-α-D-talopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1039/b916580k

Reference yield: 65.0%

: 1207163-07-2
phenyl 6-O-(tert-butyldiphenylsilyl)-3,4-O-isopropylidene-1-thio-α-D-talopyranoside

: 108-24-7
acetic anhydride

: 1207163-08-3
phenyl 2,3,4,6-tetra-O-acetyl-1-thio-α-D-talopyranoside

: 1207163-09-4
phenyl 2,3,4-tri-Oacetyl-6-O-tert-butyldiphenylsilyl-1-thio-α-D-talopyranoside

Guidance literature:: phenyl 6-O-(tert-butyldiphenylsilyl)-3,4-O-isopropylidene-1-thio-α-D-talopyranoside; With water; acetic acid; at 50 ℃; for 1h; Inert atmosphere;

acetic anhydride; With pyridine; dmap; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/b916580k