methyl (S)-3-O-dimethoxytrityl-2-O-((E)-3-phenyl-2-propen-1-yl)-glycerate

Base Information

Chemical Name:methyl (S)-3-O-dimethoxytrityl-2-O-((E)-3-phenyl-2-propen-1-yl)-glycerate
CAS No.:402856-14-8
Molecular Formula:C₃₄H₃₄O₆
Molecular Weight:538.64
Hs Code.:

Synonyms:methyl (S)-3-O-dimethoxytrityl-2-O-((E)-3-phenyl-2-propen-1-yl)-glycerate

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Chemical Property of methyl (S)-3-O-dimethoxytrityl-2-O-((E)-3-phenyl-2-propen-1-yl)-glycerate

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Technology Process of methyl (S)-3-O-dimethoxytrityl-2-O-((E)-3-phenyl-2-propen-1-yl)-glycerate

There total 3 articles about methyl (S)-3-O-dimethoxytrityl-2-O-((E)-3-phenyl-2-propen-1-yl)-glycerate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 402856-14-8
methyl (S)-3-O-dimethoxytrityl-2-O-((E)-3-phenyl-2-propen-1-yl)-glycerate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / pyridine / tetrahydrofuran / 16 h / -5 °C

2: 91 percent / Ag₂O / diethyl ether / Heating

3: bis(c-Hex₃P)benzilidine ruthenium(IV) dichloride / 1,2-dichloro-ethane / 72 h / 20 °C

With pyridine; silver(l) oxide; Grubbs catalyst first generation; In tetrahydrofuran; diethyl ether; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4020(01)00988-7

Reference yield:

: 132446-39-0
3-O-dimethoxytrityl-(S)-glyceric acid methyl ester

: 402856-14-8
methyl (S)-3-O-dimethoxytrityl-2-O-((E)-3-phenyl-2-propen-1-yl)-glycerate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / Ag₂O / diethyl ether / Heating

2: bis(c-Hex₃P)benzilidine ruthenium(IV) dichloride / 1,2-dichloro-ethane / 72 h / 20 °C

With silver(l) oxide; Grubbs catalyst first generation; In diethyl ether; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4020(01)00988-7