C₁₅H₁₃N

Base Information

• Chemical Name: C₁₅H₁₃N
• CAS No.: 1072123-53-5
• Molecular Formula: C₁₅H₁₃N
• Molecular Weight: 207.275
• Mol file: 1072123-53-5.mol

Synonyms:C₁₅H₁₃N

Chemical Property of C₁₅H₁₃N

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₁₅H₁₃N

There total 2 articles about C₁₅H₁₃N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

2-ethynylaniline (52670-38-9) + ortho-methylphenyl iodide (615-37-2) → C15H13N (1072123-53-5)

Guidance literature:

With copper(l) iodide; diethylamine; triphenylphosphine; palladium dichloride; at 40 ℃; for 24h; Inert atmosphere;

DOI:10.1021/acs.orglett.1c02449

Reference yield:

1-ethynyl-2-methylbenzene (766-47-2) + 2-iodophenylamine (615-43-0) → C15H13N (1072123-53-5)

Guidance literature:

Inert atmosphere;

DOI:10.1021/ol801844w

Reference yield: 87.0%

Thiram (137-26-8,93196-73-7) + C15H13N (1072123-53-5) → (Z)-N,N-dimethyl-4-(2-methylbenzylidene)-4H-benzo[d][1,3]thiazin-2-amine (1236003-91-0)

Guidance literature:

With silver tetrafluoroborate; In dimethyl sulfoxide; at 80 ℃; for 36h; optical yield given as %de;

DOI:10.1055/s-0029-1219828

upstream raw materials:

1-ethynyl-2-methylbenzene

2-iodophenylamine

2-ethynylaniline

ortho-methylphenyl iodide

Downstream raw materials:

(Z)-N,N-dimethyl-4-(2-methylbenzylidene)-4H-benzo[d][1,3]thiazin-2-amine

2-o-tolyl-1H-indole

5,10-di-o-tolyl-indeno[2,1-a]indene