7-(4-fluoro-benzyl)-5-methoxy-6-methyl-9-triisopropylsilanyloxy-6,7-dihydro-pyrrolo[3,4-g]quinolin-8-one

Base Information

Chemical Name:7-(4-fluoro-benzyl)-5-methoxy-6-methyl-9-triisopropylsilanyloxy-6,7-dihydro-pyrrolo[3,4-g]quinolin-8-one
CAS No.:906459-23-2
Molecular Formula:C₂₉H₃₇FN₂O₃Si
Molecular Weight:508.708
Hs Code.:

7-(4-fluoro-benzyl)-5-methoxy-6-methyl-9-triisopropylsilanyloxy-6,7-dihydro-pyrrolo[3,4-<i>g</i>]quinolin-8-one

Synonyms:7-(4-fluoro-benzyl)-5-methoxy-6-methyl-9-triisopropylsilanyloxy-6,7-dihydro-pyrrolo[3,4-g]quinolin-8-one

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Chemical Property of 7-(4-fluoro-benzyl)-5-methoxy-6-methyl-9-triisopropylsilanyloxy-6,7-dihydro-pyrrolo[3,4-g]quinolin-8-one

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Technology Process of 7-(4-fluoro-benzyl)-5-methoxy-6-methyl-9-triisopropylsilanyloxy-6,7-dihydro-pyrrolo[3,4-g]quinolin-8-one

There total 5 articles about 7-(4-fluoro-benzyl)-5-methoxy-6-methyl-9-triisopropylsilanyloxy-6,7-dihydro-pyrrolo[3,4-g]quinolin-8-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 684284-42-2
7-(4-fluoro-benzyl)-6-hydroxy-5-methoxy-6-methyl-9-triisopropylsilanyloxy-pyrrolo[3,4-g]quinoin-8-one

: 906459-23-2
7-(4-fluoro-benzyl)-5-methoxy-6-methyl-9-triisopropylsilanyloxy-6,7-dihydro-pyrrolo[3,4-g]quinolin-8-one

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/j.bmcl.2006.05.008

Reference yield:

: 684284-29-5
7-(4-fluoro-benzyl)-5,9-dihydroxy-pyrrolo[3,4-g]quinoline-6,8-dione

: 906459-23-2
7-(4-fluoro-benzyl)-5-methoxy-6-methyl-9-triisopropylsilanyloxy-6,7-dihydro-pyrrolo[3,4-g]quinolin-8-one

Guidance literature:: Multi-step reaction with 4 steps

1: imidazole / dimethylformamide / 36 h

2: K₂CO₃ / acetonitrile / 5 h / 40 °C

3: 99 percent / tetrahydrofuran; diethyl ether / 2 h / 20 °C

4: 99 percent / BF₃*OEt₂; triethylsilane / CH₂Cl₂ / 24 h / 20 °C

With 1H-imidazole; triethylsilane; boron trifluoride diethyl etherate; potassium carbonate; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2006.05.008

Reference yield:

: 684284-39-7
7-(4-fluoro-benzyl)-5-methoxy-9-triisopropylsilanyloxy-pyrrolo[3,4-g]quinoine-6,8-dione

: 906459-23-2
7-(4-fluoro-benzyl)-5-methoxy-6-methyl-9-triisopropylsilanyloxy-6,7-dihydro-pyrrolo[3,4-g]quinolin-8-one

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / tetrahydrofuran; diethyl ether / 2 h / 20 °C

2: 99 percent / BF₃*OEt₂; triethylsilane / CH₂Cl₂ / 24 h / 20 °C

With triethylsilane; boron trifluoride diethyl etherate; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.bmcl.2006.05.008