tert-butylphosphonic acid di(4-fluorophenyl) ester

Base Information

Chemical Name:tert-butylphosphonic acid di(4-fluorophenyl) ester
CAS No.:1224895-72-0
Molecular Formula:C₁₆H₁₇F₂O₃P
Molecular Weight:326.28
Hs Code.:

Synonyms:tert-butylphosphonic acid di(4-fluorophenyl) ester

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Chemical Property of tert-butylphosphonic acid di(4-fluorophenyl) ester

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Technology Process of tert-butylphosphonic acid di(4-fluorophenyl) ester

There total 1 articles about tert-butylphosphonic acid di(4-fluorophenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 371-41-5
4-Fluorophenol

: 4707-95-3
tert-butyl phosphinyl dichloride

: 1224895-72-0
tert-butylphosphonic acid di(4-fluorophenyl) ester

Guidance literature:: 4-Fluorophenol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h;

tert-butyl phosphinyl dichloride; In tetrahydrofuran;
DOI:10.1002/adsc.200900304

Reference yield: 30.4%

: 1224895-72-0
tert-butylphosphonic acid di(4-fluorophenyl) ester

: 1224895-82-2
4-fluorophenyl tert-butyl(5-fluoro-2-hydroxyphenyl)phosphinate

Guidance literature:: tert-butylphosphonic acid di(4-fluorophenyl) ester; With n-butyllithium; In tetrahydrofuran; at -78 - 20 ℃;

With hydrogenchloride; In tetrahydrofuran; water;
DOI:10.1002/adsc.200900304

Reference yield:

: 1224895-72-0
tert-butylphosphonic acid di(4-fluorophenyl) ester

: 1224895-37-7
4-fluorophenyl tert-butyl(5-fluoro-2-vinyloxyphenyl)phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran / -78 - 20 °C

2: pyridine; oxygen; copper diacetate / dichloromethane / 40 h / 20 °C

With pyridine; n-butyllithium; oxygen; copper diacetate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/adsc.200900304