Acetic acid 6-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-6-oxo-hexyl ester

Base Information

Chemical Name:Acetic acid 6-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-6-oxo-hexyl ester
CAS No.:104966-91-8
Molecular Formula:C₁₇H₂₄O₆
Molecular Weight:324.374
Hs Code.:

Synonyms:Acetic acid 6-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-6-oxo-hexyl ester

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Chemical Property of Acetic acid 6-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-6-oxo-hexyl ester

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Technology Process of Acetic acid 6-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-6-oxo-hexyl ester

There total 4 articles about Acetic acid 6-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-6-oxo-hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 502-44-3,24980-41-4,80137-66-2
hexahydro-2H-oxepin-2-one

: 104966-91-8
Acetic acid 6-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-6-oxo-hexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaOH / methanol / 5 h / Heating

2: 60 °C

3: PCl₅ / CH₂Cl₂ / 2 h / 25 °C

4: AlCl₃ / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h

With sodium hydroxide; aluminium trichloride; phosphorus pentachloride; In methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.33.4422

Reference yield:

: 5760-77-0
6-acetoxyhexanoic acid

: 104966-91-8
Acetic acid 6-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-6-oxo-hexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₅ / CH₂Cl₂ / 2 h / 25 °C

2: AlCl₃ / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h

With aluminium trichloride; phosphorus pentachloride; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.33.4422

Reference yield:

: 5299-61-6
6-hydroxyhexanoic acid sodium salt

: 104966-91-8
Acetic acid 6-(2-hydroxy-3,4-dimethoxy-6-methyl-phenyl)-6-oxo-hexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 60 °C

2: PCl₅ / CH₂Cl₂ / 2 h / 25 °C

3: AlCl₃ / 1,2-dichloro-ethane / 5 degC, 2 h; 20 degC, 70 h

With aluminium trichloride; phosphorus pentachloride; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.33.4422