Technology Process of C14H16O2
There total 1 articles about C14H16O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-trimethylsilanyl peroxide; trans-1,2-Diaminocyclohexane; tin(IV) chloride;
In
dichloromethane;
at 25 ℃;
for 24h;
regioselective reaction;
Inert atmosphere;
Molecular sieve;
DOI:10.1021/ol4006689
- Guidance literature:
-
With
N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane;
In
tetrahydrofuran; toluene;
at -78 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1021/ol4006689
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere
2: tetrakis(triphenylphosphine) palladium(0); triethylaluminum / 1,2-dichloro-ethane; hexane / 2 h / 0 - 25 °C / Inert atmosphere
With
N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium(0); triethylaluminum; potassium hexamethylsilazane;
In
tetrahydrofuran; hexane; 1,2-dichloro-ethane; toluene;
DOI:10.1021/ol4006689