(3-tert-Butyl-5-{4-[3-tert-butyl-5-(4-iodo-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenylethynyl)-trimethyl-silane

Base Information

Chemical Name:(3-tert-Butyl-5-{4-[3-tert-butyl-5-(4-iodo-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenylethynyl)-trimethyl-silane
CAS No.:156264-90-3
Molecular Formula:C₄₃H₄₁ISi
Molecular Weight:712.789
Hs Code.:

Synonyms:(3-tert-Butyl-5-{4-[3-tert-butyl-5-(4-iodo-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenylethynyl)-trimethyl-silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-tert-Butyl-5-{4-[3-tert-butyl-5-(4-iodo-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenylethynyl)-trimethyl-silane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (3-tert-Butyl-5-{4-[3-tert-butyl-5-(4-iodo-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenylethynyl)-trimethyl-silane

There total 6 articles about (3-tert-Butyl-5-{4-[3-tert-butyl-5-(4-iodo-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenylethynyl)-trimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 156264-88-9
C₄₇H₅₁N₃Si

: 156264-90-3
(3-tert-Butyl-5-{4-[3-tert-butyl-5-(4-iodo-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenylethynyl)-trimethyl-silane

Guidance literature:: With methyl iodide; at 110 ℃; for 12h;
DOI:10.1021/ja00089a012

Reference yield:

: 156264-85-6
C₂₇H₃₅N₃Si

: 156264-90-3
(3-tert-Butyl-5-{4-[3-tert-butyl-5-(4-iodo-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenylethynyl)-trimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / MeI / 12 h / 110 °C

2: 87 percent / Pb(dba)2, PPh₃, CuI, Et₃N / 12 h / 80 °C

3: 92 percent / MeI / 12 h / 110 °C

With copper(l) iodide; Pb(dba)2; triethylamine; triphenylphosphine; methyl iodide;
DOI:10.1021/ja00089a012

Reference yield:

: 144001-06-9
1-(trimethylsilyl)-2-(3-bromo-5-tert-butylphenyl)acetylene

: 156264-90-3
(3-tert-Butyl-5-{4-[3-tert-butyl-5-(4-iodo-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenylethynyl)-trimethyl-silane

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / Pb(dba)2, PPh₃, CuI, Et₃N / 12 h / 80 °C

2: 94 percent / MeI / 12 h / 110 °C

3: 87 percent / Pb(dba)2, PPh₃, CuI, Et₃N / 12 h / 80 °C

4: 92 percent / MeI / 12 h / 110 °C

With copper(l) iodide; Pb(dba)2; triethylamine; triphenylphosphine; methyl iodide;
DOI:10.1021/ja00089a012