3-O-allyl-2,4,6-tri-O-(p-bromobenzyl)-D-mannopyranose

Base Information

Chemical Name:3-O-allyl-2,4,6-tri-O-(p-bromobenzyl)-D-mannopyranose
CAS No.:75975-13-2
Molecular Formula:C₃₀H₃₁Br₃O₆
Molecular Weight:727.285
Hs Code.:

Synonyms:3-O-allyl-2,4,6-tri-O-(p-bromobenzyl)-D-mannopyranose

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Chemical Property of 3-O-allyl-2,4,6-tri-O-(p-bromobenzyl)-D-mannopyranose

Chemical Property:

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Technology Process of 3-O-allyl-2,4,6-tri-O-(p-bromobenzyl)-D-mannopyranose

There total 3 articles about 3-O-allyl-2,4,6-tri-O-(p-bromobenzyl)-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75962-00-4
3-O-allyl-2,4,6-tri-O-(p-bromobenzyl)-α-D-mannopyranoside

: 75975-13-2
3-O-allyl-2,4,6-tri-O-(p-bromobenzyl)-D-mannopyranose

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; water; acetic acid; for 5h; Heating;
DOI:10.1021/jo00317a030

Reference yield:

: 75962-02-6
2,4,6-Tri-O-(p-bromobenzyl)-D-mannopyranosyl Chloride

: 75975-13-2
3-O-allyl-2,4,6-tri-O-(p-bromobenzyl)-D-mannopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / NaH / tetrahydrofuran / 1 h / Heating

2: 72 percent / KOH / toluene / Heating

3: concentrated HCl / acetic acid; dioxane; H₂O / 5 h / Heating

With hydrogenchloride; potassium hydroxide; sodium hydride; In tetrahydrofuran; 1,4-dioxane; water; acetic acid; toluene;
DOI:10.1021/jo00317a030

Reference yield:

: 75962-03-7
1,3-Anhydro-2,4,6-tri-O-(p-bromobenzyl)-β-D-mannopyranose

: 75975-13-2
3-O-allyl-2,4,6-tri-O-(p-bromobenzyl)-D-mannopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / KOH / toluene / Heating

2: concentrated HCl / acetic acid; dioxane; H₂O / 5 h / Heating

With hydrogenchloride; potassium hydroxide; In 1,4-dioxane; water; acetic acid; toluene;
DOI:10.1021/jo00317a030