Methyl 5-{[(6-(benzyloxy)-5-{[(6-isopropoxy-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-6-isopropoxy-2-pyridine carboxylate

Base Information

Chemical Name:Methyl 5-{[(6-(benzyloxy)-5-{[(6-isopropoxy-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-6-isopropoxy-2-pyridine carboxylate
CAS No.:475272-87-8
Molecular Formula:C₃₂H₃₂N₆O₉
Molecular Weight:644.641
Hs Code.:

Synonyms:Methyl 5-{[(6-(benzyloxy)-5-{[(6-isopropoxy-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-6-isopropoxy-2-pyridine carboxylate

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Chemical Property of Methyl 5-{[(6-(benzyloxy)-5-{[(6-isopropoxy-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-6-isopropoxy-2-pyridine carboxylate

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Technology Process of Methyl 5-{[(6-(benzyloxy)-5-{[(6-isopropoxy-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-6-isopropoxy-2-pyridine carboxylate

There total 14 articles about Methyl 5-{[(6-(benzyloxy)-5-{[(6-isopropoxy-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-6-isopropoxy-2-pyridine carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 475272-87-8
Methyl 5-{[(6-(benzyloxy)-5-{[(6-isopropoxy-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-6-isopropoxy-2-pyridine carboxylate

Guidance literature:

Reference yield:

: 16013-85-7,136901-10-5
2,6-dicholoro-3-nitropyridine

: 475272-87-8
Methyl 5-{[(6-(benzyloxy)-5-{[(6-isopropoxy-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-6-isopropoxy-2-pyridine carboxylate

Guidance literature:: Multi-step reaction with 8 steps

1.1: NH₃ / ethanol

1.2: NaNO₂; H₂SO₄

1.3: H₂O

2.1: Ag₂CO₃

3.1: [Pd(PPh₃)4]

4.1: O₃ / acetic acid

4.2: AgNO₃; KOH

5.1: (COCl)2 / dimethylformamide

6.1: DIEA

7.1: H₂ / PtO₂

8.1: DIEA

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; oxalyl dichloride; ammonia; hydrogen; ozone; N-ethyl-N,N-diisopropylamine; silver carbonate; platinum(IV) oxide; In ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/anie.200390154

Reference yield:

: 92138-35-7
6-chloro-3-nitro-1H-pyridin-2-one

: 475272-87-8
Methyl 5-{[(6-(benzyloxy)-5-{[(6-isopropoxy-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-6-isopropoxy-2-pyridine carboxylate

Guidance literature:: Multi-step reaction with 7 steps

1.1: Ag₂CO₃

2.1: [Pd(PPh₃)4]

3.1: O₃ / acetic acid

3.2: AgNO₃; KOH

4.1: (COCl)2 / dimethylformamide

5.1: DIEA

6.1: H₂ / PtO₂

7.1: DIEA

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; oxalyl dichloride; hydrogen; ozone; N-ethyl-N,N-diisopropylamine; silver carbonate; platinum(IV) oxide; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/anie.200390154