3-(4-chloro-phenyl)-6,8-dimethyl-8H-pyrimido[5,4-e][1,2,4]triazine-5,7-dione

Base Information

• Chemical Name: 3-(4-chloro-phenyl)-6,8-dimethyl-8H-pyrimido[5,4-e][1,2,4]triazine-5,7-dione
• CAS No.: 30561-26-3
• Molecular Formula: C₁₃H₁₀ClN₅O₂
• Molecular Weight: 303.708

Synonyms:3-(4-chloro-phenyl)-6,8-dimethyl-8H-pyrimido[5,4-e][1,2,4]triazine-5,7-dione

Chemical Property of 3-(4-chloro-phenyl)-6,8-dimethyl-8H-pyrimido[5,4-e][1,2,4]triazine-5,7-dione

Chemical Property:

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Technology Process of 3-(4-chloro-phenyl)-6,8-dimethyl-8H-pyrimido[5,4-e][1,2,4]triazine-5,7-dione

There total 7 articles about 3-(4-chloro-phenyl)-6,8-dimethyl-8H-pyrimido[5,4-e][1,2,4]triazine-5,7-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

6-{N'-[1-(4-Chloro-phenyl)-meth-(Z)-ylidene]-hydrazino}-1,3-dimethyl-5-(4-nitro-phenylazo)-1H-pyrimidine-2,4-dione (78158-88-0) → 3-(4-chloro-phenyl)-6,8-dimethyl-8H-pyrimido[5,4-e][1,2,4]triazine-5,7-dione (30561-26-3)

Guidance literature:

With N,N-dimethyl-formamide dimethyl acetal; at 150 ℃; for 5h;

DOI:10.1002/jhet.5570190413

Reference yield: 56.0%

6-{N'-[1-(4-Chloro-phenyl)-meth-(Z)-ylidene]-hydrazino}-1,3-dimethyl-5-phenylazo-1H-pyrimidine-2,4-dione (78158-83-5) → 3-(4-chloro-phenyl)-6,8-dimethyl-8H-pyrimido[5,4-e][1,2,4]triazine-5,7-dione (30561-26-3)

Guidance literature:

With N,N-dimethyl-formamide dimethyl acetal; at 150 ℃; for 5h;

DOI:10.1002/jhet.5570190413

Reference yield: 56.0%

6-{N'-[1-(4-Chloro-phenyl)-meth-(Z)-ylidene]-hydrazino}-1,3-dimethyl-5-phenylazo-1H-pyrimidine-2,4-dione (78158-83-5) → C-Methoxy-N,N-dimethyl-N'-phenyl-methanediamine + 3-(4-chloro-phenyl)-6,8-dimethyl-8H-pyrimido[5,4-e][1,2,4]triazine-5,7-dione (30561-26-3)

Guidance literature:

With N,N-dimethyl-formamide dimethyl acetal; at 150 ℃; for 5h;

upstream raw materials:

6-{N'-[1-(4-Chloro-phenyl)-meth-(Z)-ylidene]-hydrazino}-1,3-dimethyl-5-phenylazo-1H-pyrimidine-2,4-dione

6-{N'-[1-(4-Chloro-phenyl)-meth-(Z)-ylidene]-hydrazino}-1,3-dimethyl-5-(4-nitro-phenylazo)-1H-pyrimidine-2,4-dione

phenylpropynoic acid ethyl ester

3-(4-chloro-phenyl)-6,8-dimethyl-4-oxy-8H-pyrimido[5,4-e][1,2,4]triazine-5,7-dione

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