Technology Process of C7H10O2
There total 1 articles about C7H10O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trimethylamine-N-oxide / 8 h / -15 - 20 °C
2: 1H-imidazole; dmap / N,N-dimethyl-formamide / 1 h / 80 °C
3: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 1 h / -20 °C
4: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 12 h / Reflux
With
1H-imidazole; dmap; sodium tetrahydroborate; trimethylamine-N-oxide; cerium(III) chloride heptahydrate; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
1: Pauson-Khand reaction / 3: Luche reduction;
DOI:10.1016/j.tetlet.2012.06.059
- Guidance literature:
-
Multi-step reaction with 5 steps
1: trimethylamine-N-oxide / 8 h / -15 - 20 °C
2: 1H-imidazole; dmap / N,N-dimethyl-formamide / 1 h / 80 °C
3: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 1 h / -20 °C
4: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 12 h / Reflux
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 20 °C
With
1H-imidazole; dmap; sodium tetrahydroborate; trimethylamine-N-oxide; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
1: Pauson-Khand reaction / 3: Luche reduction;
DOI:10.1016/j.tetlet.2012.06.059
