8,19-Bis-(toluene-4-sulfonyl)-7,8,9,10,17,18,19,20,21,22-decahydro-6H,16H-5,11-dioxa-8,16,19,22-tetraaza-dibenzo[a,j]cyclooctadecene

Base Information

Chemical Name:8,19-Bis-(toluene-4-sulfonyl)-7,8,9,10,17,18,19,20,21,22-decahydro-6H,16H-5,11-dioxa-8,16,19,22-tetraaza-dibenzo[a,j]cyclooctadecene
CAS No.:109888-84-8
Molecular Formula:C₃₄H₄₀N₄O₆S₂
Molecular Weight:664.847
Hs Code.:

Synonyms:8,19-Bis-(toluene-4-sulfonyl)-7,8,9,10,17,18,19,20,21,22-decahydro-6H,16H-5,11-dioxa-8,16,19,22-tetraaza-dibenzo[a,j]cyclooctadecene

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Chemical Property of 8,19-Bis-(toluene-4-sulfonyl)-7,8,9,10,17,18,19,20,21,22-decahydro-6H,16H-5,11-dioxa-8,16,19,22-tetraaza-dibenzo[a,j]cyclooctadecene

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Technology Process of 8,19-Bis-(toluene-4-sulfonyl)-7,8,9,10,17,18,19,20,21,22-decahydro-6H,16H-5,11-dioxa-8,16,19,22-tetraaza-dibenzo[a,j]cyclooctadecene

There total 5 articles about 8,19-Bis-(toluene-4-sulfonyl)-7,8,9,10,17,18,19,20,21,22-decahydro-6H,16H-5,11-dioxa-8,16,19,22-tetraaza-dibenzo[a,j]cyclooctadecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 120340-69-4
8,19-Bis-(toluene-4-sulfonyl)-7,8,9,10,19,20-hexahydro-6H,16H,18H,22H-5,11-dioxa-8,16,19,22-tetraaza-dibenzo[a,j]cyclooctadecene-17,21-dione

: 109888-84-8
8,19-Bis-(toluene-4-sulfonyl)-7,8,9,10,17,18,19,20,21,22-decahydro-6H,16H-5,11-dioxa-8,16,19,22-tetraaza-dibenzo[a,j]cyclooctadecene

Guidance literature:: With diborane; In tetrahydrofuran;
DOI:10.1007/BF00479353

Reference yield:

: 42031-77-6
N-Tosyliminodiacetic acid dichloroanhydride

: 109888-84-8
8,19-Bis-(toluene-4-sulfonyl)-7,8,9,10,17,18,19,20,21,22-decahydro-6H,16H-5,11-dioxa-8,16,19,22-tetraaza-dibenzo[a,j]cyclooctadecene

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / pyridine / dioxane; benzene / 6 h / 75 °C

2: 77 percent / B₂H₆ / tetrahydrofuran

With pyridine; diborane; In tetrahydrofuran; 1,4-dioxane; benzene;
DOI:10.1007/BF00479353

Reference yield:

: 54533-68-5
1,5-bis(2-aminophenoxy)-3-(4-toluenesulfonyl)-3-azapentane

: 109888-84-8
8,19-Bis-(toluene-4-sulfonyl)-7,8,9,10,17,18,19,20,21,22-decahydro-6H,16H-5,11-dioxa-8,16,19,22-tetraaza-dibenzo[a,j]cyclooctadecene

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / pyridine / dioxane; benzene / 6 h / 75 °C

2: 77 percent / B₂H₆ / tetrahydrofuran

With pyridine; diborane; In tetrahydrofuran; 1,4-dioxane; benzene;
DOI:10.1007/BF00479353