1,3-diphenyl<4,5,6,7,8,9,10,11-2H8>cyclopentaphenanthren-2-one

Base Information

• Chemical Name: 1,3-diphenyl<4,5,6,7,8,9,10,11-2H8>cyclopentaphenanthren-2-one
• CAS No.: 113474-60-5
• Molecular Formula: C₂₉H₁₈O
• Molecular Weight: 390.398

Synonyms:1,3-diphenyl<4,5,6,7,8,9,10,11-2H8>cyclopentaphenanthren-2-one

Chemical Property of 1,3-diphenyl<4,5,6,7,8,9,10,11-2H8>cyclopentaphenanthren-2-one

Chemical Property:

Purity/Quality:

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Technology Process of 1,3-diphenyl<4,5,6,7,8,9,10,11-2H8>cyclopentaphenanthren-2-one

There total 2 articles about 1,3-diphenyl<4,5,6,7,8,9,10,11-2H8>cyclopentaphenanthren-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

<2H8>-phenanthrene-9,10-quinone (113451-49-3) + 1,3-Diphenylpropanone (102-04-5) → 1,3-diphenyl<4,5,6,7,8,9,10,11-2H8>cyclopentaphenanthren-2-one (113474-60-5)

Guidance literature:

With potassium hydroxide; In ethanol; for 0.0833333h; Heating;

DOI:10.1021/jo00243a016

Reference yield:

decadeuterio-phenanthrene (1517-22-2) → 1,3-diphenyl<4,5,6,7,8,9,10,11-2H8>cyclopentaphenanthren-2-one (113474-60-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 84 percent / CrO₃, aq. AcOH / 0.5 h / 60 °C

2: 50 percent / KOH / ethanol / 0.08 h / Heating

With chromium(VI) oxide; potassium hydroxide; acetic acid; In ethanol;

DOI:10.1021/jo00243a016

Reference yield: 35.0%

1,3-diphenyl<4,5,6,7,8,9,10,11-2H8>cyclopentaphenanthren-2-one (113474-60-5) + diphenyl acetylene (501-65-5) → 1,2,3,4-tetraphenyl<5,6,7,8,9,10,11,12-2H8>triphenylene (113451-50-6)

Guidance literature:

at 300 ℃; for 2h;

DOI:10.1021/jo00243a016

upstream raw materials:

<2H8>-phenanthrene-9,10-quinone

1,3-Diphenylpropanone

decadeuterio-phenanthrene

Downstream raw materials:

1,2,3,4-tetraphenyl<5,6,7,8,9,10,11,12-2H8>triphenylene

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