1D-3-O-benzyl-1,2:4,5-di-O-cyclohexylidene-6-O-(4-methoxybenzyl)-myo-inositol

Base Information

Chemical Name:1D-3-O-benzyl-1,2:4,5-di-O-cyclohexylidene-6-O-(4-methoxybenzyl)-myo-inositol
CAS No.:170555-90-5
Molecular Formula:C₃₃H₄₂O₇
Molecular Weight:550.692
Hs Code.:

Synonyms:1D-3-O-benzyl-1,2:4,5-di-O-cyclohexylidene-6-O-(4-methoxybenzyl)-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1D-3-O-benzyl-1,2:4,5-di-O-cyclohexylidene-6-O-(4-methoxybenzyl)-myo-inositol

Chemical Property:

Purity/Quality:

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Technology Process of 1D-3-O-benzyl-1,2:4,5-di-O-cyclohexylidene-6-O-(4-methoxybenzyl)-myo-inositol

There total 1 articles about 1D-3-O-benzyl-1,2:4,5-di-O-cyclohexylidene-6-O-(4-methoxybenzyl)-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 23393-20-6,111901-82-7,120202-94-0,134109-10-7,134109-11-8,136375-66-1,126722-28-9
1D-3-O-benzyl-1,2:4,5-di-O-cyclohexylidene-myo-inositol

: 824-94-2
p-methoxybenzyl chloride

: 170555-90-5
1D-3-O-benzyl-1,2:4,5-di-O-cyclohexylidene-6-O-(4-methoxybenzyl)-myo-inositol

Guidance literature:: With sodium hydride; potassium iodide; In N,N-dimethyl-formamide; for 1.5h; Ambient temperature;
DOI:10.1016/0008-6215(95)00012-I

Reference yield: 57.0%

: 170555-90-5
1D-3-O-benzyl-1,2:4,5-di-O-cyclohexylidene-6-O-(4-methoxybenzyl)-myo-inositol

: 170555-91-6
1D-3-O-benzyl-1,2-O-cyclohexylidene-6-O-(4-methoxybenzyl)-myo-inositol

Guidance literature:: With toluene-4-sulfonic acid; In chloroform; ethylene glycol; acetonitrile; for 0.333333h; Ambient temperature;
DOI:10.1016/0008-6215(95)00012-I

Reference yield:

: 170555-90-5
1D-3-O-benzyl-1,2:4,5-di-O-cyclohexylidene-6-O-(4-methoxybenzyl)-myo-inositol

: 133076-45-6
O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3,4,5-tetra-O-benzyl-D-myo-inositol

Guidance literature:: Multi-step reaction with 7 steps

1: 57 percent / p-toluenesulfonic acid / ethane-1,2-diol; CHCl₃; acetonitrile / 0.33 h / Ambient temperature

2: NaH / dimethylformamide / Ambient temperature

3: BF₃*Et₂O / CH₂Cl₂ / 0.08 h / Ambient temperature

4: 1.) 3A molecular sieves, trimethylsilyl trifluoromethanesulfonate, 2.) 42percent aq. tetrafluoroboric acid / 1.) Et₂O, CH₂Cl₂, -55 deg C, 0.5 h, 2.) MeCN, RT, 0.5 h

5: 1.) dibutyltin oxide, 2.) KI, CsF / 1.) MeOH, reflux, 2 h, 2.) DMF, RT, overnight

6: NaH / dimethylformamide / 1 h / Ambient temperature

7: CF₃COOH / CH₂Cl₂ / 1 h / Ambient temperature

With tetrafluoroboric acid; trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; boron trifluoride diethyl etherate; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; cesium fluoride; trifluoroacetic acid; potassium iodide; In dichloromethane; chloroform; ethylene glycol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0008-6215(95)00012-I