C₄₅H₇₃N₃O₁₂

Base Information

Chemical Name:C₄₅H₇₃N₃O₁₂
CAS No.:1384974-69-9
Molecular Formula:C₄₅H₇₃N₃O₁₂
Molecular Weight:848.088
Hs Code.:

C<sub>45</sub>H<sub>73</sub>N<sub>3</sub>O<sub>12</sub>

Synonyms:C₄₅H₇₃N₃O₁₂

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Chemical Property of C₄₅H₇₃N₃O₁₂

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Technology Process of C₄₅H₇₃N₃O₁₂

There total 10 articles about C₄₅H₇₃N₃O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: C₁₈H₂₇NO₄*ClH

: 1384974-67-7
C₂₇H₄₈N₂O₉

: 1384974-69-9
C₄₅H₇₃N₃O₁₂

Guidance literature:: C₂₇H₄₈N₂O₉; With 1-chloro-1-(dimethylamino)-2-methyl-1-propene; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

C₁₈H₂₇NO₄*ClH; With N-ethyl-N,N-diisopropylamine; In dichloromethane; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.05.110

Reference yield:

: 22838-58-0
Boc-D-Val-OH

: 1384974-69-9
C₄₅H₇₃N₃O₁₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

1.2: pH 2

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C / Inert atmosphere

3.1: hydrogenchloride / 1,4-dioxane / Inert atmosphere

4.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

4.2: Inert atmosphere

With hydrogenchloride; dmap; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; 1,4-dioxane; dichloromethane; mineral oil;
DOI:10.1016/j.tetlet.2012.05.110

Reference yield:

: 2441-07-8,65138-05-8,14487-24-2
benzyl (R)-2-hydroxy-3-methylbutanoate

: 1384974-69-9
C₄₅H₇₃N₃O₁₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C / Inert atmosphere

2.1: hydrogenchloride / 1,4-dioxane / Inert atmosphere

3.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

3.2: Inert atmosphere

With hydrogenchloride; dmap; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.tetlet.2012.05.110