(S)-3-(4-methoxyphenyl)-2-((S)-2-(2-morpholinoacetamido)propionamido)propionic acid methyl ester

Base Information

Chemical Name:(S)-3-(4-methoxyphenyl)-2-((S)-2-(2-morpholinoacetamido)propionamido)propionic acid methyl ester
CAS No.:1620107-79-0
Molecular Formula:C₂₀H₂₉N₃O₆
Molecular Weight:407.467
Hs Code.:

Synonyms:(S)-3-(4-methoxyphenyl)-2-((S)-2-(2-morpholinoacetamido)propionamido)propionic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-(4-methoxyphenyl)-2-((S)-2-(2-morpholinoacetamido)propionamido)propionic acid methyl ester

Chemical Property:

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Technology Process of (S)-3-(4-methoxyphenyl)-2-((S)-2-(2-morpholinoacetamido)propionamido)propionic acid methyl ester

There total 5 articles about (S)-3-(4-methoxyphenyl)-2-((S)-2-(2-morpholinoacetamido)propionamido)propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3235-69-6
morpholin-4-ylacetic acid

: 1598434-36-6
C₁₄H₂₀N₂O₄*C₂HF₃O₂

: 1620107-79-0
(S)-3-(4-methoxyphenyl)-2-((S)-2-(2-morpholinoacetamido)propionamido)propionic acid methyl ester

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; for 1h;
DOI:10.1016/j.ejmech.2021.113267

Reference yield:

: 3235-69-6
morpholin-4-ylacetic acid

: (S)-2-((S)-2-aminopropionamido)-3-(4-methoxyphenyl)propionic acid methyl ester hydrochloride

: 1620107-79-0
(S)-3-(4-methoxyphenyl)-2-((S)-2-(2-morpholinoacetamido)propionamido)propionic acid methyl ester

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; water; at 20 ℃; for 2h;

Reference yield:

: 7479-01-8
O-methyl-L-tyrosine methyl ester hydrochloride

: 1620107-79-0
(S)-3-(4-methoxyphenyl)-2-((S)-2-(2-morpholinoacetamido)propionamido)propionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 2-(6-chloro-1H-benzotriazole-1-yl)21,1,3,3-tetramethylaminiumhexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h

2: 0.5 h

3: 2-(6-chloro-1H-benzotriazole-1-yl)21,1,3,3-tetramethylaminiumhexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane

With 2-(6-chloro-1H-benzotriazole-1-yl)21,1,3,3-tetramethylaminiumhexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm500716s