C₄₀H₅₄N₄O₈S

Base Information

Chemical Name:C₄₀H₅₄N₄O₈S
CAS No.:1079399-08-8
Molecular Formula:C₄₀H₅₄N₄O₈S
Molecular Weight:750.957
Hs Code.:

C<sub>40</sub>H<sub>54</sub>N<sub>4</sub>O<sub>8</sub>S

Synonyms:C₄₀H₅₄N₄O₈S

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Chemical Property of C₄₀H₅₄N₄O₈S

Chemical Property:

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Technology Process of C₄₀H₅₄N₄O₈S

There total 18 articles about C₄₀H₅₄N₄O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₀H₅₂N₄O₈S

: 1079399-08-8
C₄₀H₅₄N₄O₈S

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 25 ℃; under 759.826 Torr;

Reference yield:

: 2398-37-0
3-methoxyphenyl bromide

: 1079399-08-8
C₄₀H₅₄N₄O₈S

Guidance literature:: Multi-step reaction with 13 steps

1.1: magnesium / iodine / tetrahydrofuran / 4 h / Heating / reflux

2.1: boron tribromide / dichloromethane / 3 h / 0 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 17 h / 20 - 110 °C

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.25 h / -15 °C

4.2: 12.5 h / -15 - 20 °C

5.1: hydrogenchloride / 3 h / 0 - 20 °C

6.1: silver(l) oxide / N,N-dimethyl-formamide / 14 h / 20 °C

7.1: sulfuric acid; water / 1,4-dioxane / 3 h / 20 °C / Heating / reflux

8.1: dipyridinium dichromate / dichloromethane / 10 h / 0 - 20 °C / Molecular sieve

9.1: 2-hydroxypyridin; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 h / 70 °C

10.1: triphenylphosphine / methanol; water / 17 h

11.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.25 h / 0 °C

11.2: 16.17 h / 0 - 20 °C

12.1: Hoveyda-Grubbs catalyst second generation / 1,2-dichloro-ethane / 90 °C

13.1: hydrogen / palladium on activated charcoal / ethanol / 25 °C / 759.83 Torr

With 2-hydroxypyridin; hydrogenchloride; dipyridinium dichromate; di-isopropyl azodicarboxylate; sulfuric acid; water; hydrogen; boron tribromide; potassium carbonate; magnesium; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; silver(l) oxide; Hoveyda-Grubbs catalyst second generation; palladium on activated charcoal; iodine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 5-[2-(3-allyl-phenoxy)-1-azido-ethyl]-3-methoxy-tetrahydro-furan-2-ol

: 1079399-08-8
C₄₀H₅₄N₄O₈S

Guidance literature:: Multi-step reaction with 6 steps

1.1: dipyridinium dichromate / dichloromethane / 10 h / 0 - 20 °C / Molecular sieve

2.1: 2-hydroxypyridin; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 h / 70 °C

3.1: triphenylphosphine / methanol; water / 17 h

4.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.25 h / 0 °C

4.2: 16.17 h / 0 - 20 °C

5.1: Hoveyda-Grubbs catalyst second generation / 1,2-dichloro-ethane / 90 °C

6.1: hydrogen / palladium on activated charcoal / ethanol / 25 °C / 759.83 Torr

With 2-hydroxypyridin; dipyridinium dichromate; hydrogen; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; Hoveyda-Grubbs catalyst second generation; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;