N-(6-bromo-4-isopropoxy-2-methoxy-3-methylbenzyl)-N-(2,2-dimethoxyethylidene)amine

Base Information

• Chemical Name: N-(6-bromo-4-isopropoxy-2-methoxy-3-methylbenzyl)-N-(2,2-dimethoxyethylidene)amine
• CAS No.: 898828-47-2
• Molecular Formula: C₁₆H₂₆BrNO₄
• Molecular Weight: 376.291

Synonyms:N-(6-bromo-4-isopropoxy-2-methoxy-3-methylbenzyl)-N-(2,2-dimethoxyethylidene)amine

Chemical Property of N-(6-bromo-4-isopropoxy-2-methoxy-3-methylbenzyl)-N-(2,2-dimethoxyethylidene)amine

Chemical Property:

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Technology Process of N-(6-bromo-4-isopropoxy-2-methoxy-3-methylbenzyl)-N-(2,2-dimethoxyethylidene)amine

There total 2 articles about N-(6-bromo-4-isopropoxy-2-methoxy-3-methylbenzyl)-N-(2,2-dimethoxyethylidene)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(6-Bromo-4-isopropoxy-2-methoxy-3-methyl-benzyl)-[2,2-dimethoxy-eth-(E)-ylidene]-amine → N-(6-bromo-4-isopropoxy-2-methoxy-3-methylbenzyl)-N-(2,2-dimethoxyethylidene)amine (898828-47-2)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 2h;

DOI:10.1016/j.tet.2006.03.076

Reference yield:

6-bromo-4-isopropoxy-2-methoxy-3-methylbenzaldehyde (863647-50-1) → N-(6-bromo-4-isopropoxy-2-methoxy-3-methylbenzyl)-N-(2,2-dimethoxyethylidene)amine (898828-47-2)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 3 h / Heating

2: 1.91 g / NaBH₄ / methanol / 2 h / 20 °C

With sodium tetrahydroborate; In methanol; toluene;

DOI:10.1016/j.tet.2006.03.076

Reference yield: 70.0%

N-(6-bromo-4-isopropoxy-2-methoxy-3-methylbenzyl)-N-(2,2-dimethoxyethylidene)amine (898828-47-2) + methyl chloroformate (79-22-1) → methyl N-(6-bromo-4-isopropoxy-2-methoxy-3-methylbenzyl)-N-(2,2-dimethoxyethyl)carbamate (898828-45-0)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;

DOI:10.1016/j.tet.2006.03.076

upstream raw materials:

6-bromo-4-isopropoxy-2-methoxy-3-methylbenzaldehyde

Downstream raw materials:

methyl N-(6-bromo-4-isopropoxy-2-methoxy-3-methylbenzyl)-N-(2,2-dimethoxyethyl)carbamate

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