N-Ethyl-N-[4-(3,4-dimethoxybenzoyloxy)butyl]-6,7-dimethoxy-1,2,3,4-tetrahydro-2-naphthylamine

Base Information

Chemical Name:N-Ethyl-N-[4-(3,4-dimethoxybenzoyloxy)butyl]-6,7-dimethoxy-1,2,3,4-tetrahydro-2-naphthylamine
CAS No.:82763-60-8
Molecular Formula:C₂₇H₃₇NO₆
Molecular Weight:471.594
Hs Code.:

Synonyms:N-Ethyl-N-[4-(3,4-dimethoxybenzoyloxy)butyl]-6,7-dimethoxy-1,2,3,4-tetrahydro-2-naphthylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Ethyl-N-[4-(3,4-dimethoxybenzoyloxy)butyl]-6,7-dimethoxy-1,2,3,4-tetrahydro-2-naphthylamine

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Technology Process of N-Ethyl-N-[4-(3,4-dimethoxybenzoyloxy)butyl]-6,7-dimethoxy-1,2,3,4-tetrahydro-2-naphthylamine

There total 4 articles about N-Ethyl-N-[4-(3,4-dimethoxybenzoyloxy)butyl]-6,7-dimethoxy-1,2,3,4-tetrahydro-2-naphthylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 82763-29-9
2-(N-ethyl)amino-6,7-dimethoxy tetraline

: 69788-75-6
3,4-Dimethoxy-benzoic acid 4-chloro-butyl ester

: 82763-60-8
N-Ethyl-N-[4-(3,4-dimethoxybenzoyloxy)butyl]-6,7-dimethoxy-1,2,3,4-tetrahydro-2-naphthylamine

Guidance literature:: With sodium carbonate; sodium iodide; In butanone; for 96h; Heating;
DOI:10.1021/jm00353a016

Reference yield:

: 69788-75-6
3,4-Dimethoxy-benzoic acid 4-chloro-butyl ester

: 69788-74-5
N-ethyl-6,7-dimethoxy-1,2,3,4-tetrahydro-2-naphthylamine hydrochloride

: 82763-60-8
N-Ethyl-N-[4-(3,4-dimethoxybenzoyloxy)butyl]-6,7-dimethoxy-1,2,3,4-tetrahydro-2-naphthylamine

Guidance literature:: Multistep reaction; (i) aq. NaOH, (ii) /BRN= 2978736/, NaI, Na₂CO₃, MeCOEt;

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 82763-60-8
N-Ethyl-N-[4-(3,4-dimethoxybenzoyloxy)butyl]-6,7-dimethoxy-1,2,3,4-tetrahydro-2-naphthylamine

Guidance literature:: Multi-step reaction with 3 steps

1: PCl₅ / CH₂Cl₂

2: 1.) AlCl₃, 2.) H₂ / PtO₂ / 1.) CH₂Cl₂, RT, 4 h, 2.) EtOH, 1 atm

3: 59 percent / NaI, Na₂CO₃ / butan-2-one / 96 h / Heating

With aluminium trichloride; phosphorus pentachloride; hydrogen; sodium carbonate; sodium iodide; platinum(IV) oxide; In dichloromethane; butanone;
DOI:10.1021/jm00353a016