Technology Process of C30H28O3S3
There total 7 articles about C30H28O3S3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanol; potassium carbonate;
In
chloroform;
at 20 ℃;
for 3h;
DOI:10.1021/jo070607z
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 100 percent / PPh3; CuI; triethylamine / PdCl2 / 6 h / 20 °C
2: 98 percent / potassium carbonate; methanol / CH2Cl2 / 6 h / 20 °C
3: 58 percent / triethylamine; CuI / Pd(PPh3)2Cl2 / tetrahydrofuran / 20 °C
4: 87 percent / triethylamine; CuI / Pd(PPh3)2Cl2 / tetrahydrofuran / 6 h / 20 °C
5: 92 percent / potassium carbonate; methanol / CHCl3 / 3 h / 20 °C
With
methanol; copper(l) iodide; potassium carbonate; triethylamine; triphenylphosphine;
bis-triphenylphosphine-palladium(II) chloride; palladium dichloride;
In
tetrahydrofuran; dichloromethane; chloroform;
1: Sonogashira coupling / 3: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1021/jo070607z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 87 percent / triethylamine; CuI / Pd(PPh3)2Cl2 / tetrahydrofuran / 6 h / 20 °C
2: 92 percent / potassium carbonate; methanol / CHCl3 / 3 h / 20 °C
With
methanol; copper(l) iodide; potassium carbonate; triethylamine;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran; chloroform;
1: Sonogashira coupling;
DOI:10.1021/jo070607z
