N-(pyridin-2-ylmethyl)-N-(diphenylphosphanyl)-1,1-diphenylphosphanamine

Base Information

Chemical Name:N-(pyridin-2-ylmethyl)-N-(diphenylphosphanyl)-1,1-diphenylphosphanamine
CAS No.:1015762-93-2
Molecular Formula:C₃₀H₂₆N₂P₂
Molecular Weight:476.497
Hs Code.:

Synonyms:N-(pyridin-2-ylmethyl)-N-(diphenylphosphanyl)-1,1-diphenylphosphanamine

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Chemical Property of N-(pyridin-2-ylmethyl)-N-(diphenylphosphanyl)-1,1-diphenylphosphanamine

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Technology Process of N-(pyridin-2-ylmethyl)-N-(diphenylphosphanyl)-1,1-diphenylphosphanamine

There total 2 articles about N-(pyridin-2-ylmethyl)-N-(diphenylphosphanyl)-1,1-diphenylphosphanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3731-51-9
2-(Aminomethyl)pyridine

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1015762-93-2
N-(pyridin-2-ylmethyl)-N-(diphenylphosphanyl)-1,1-diphenylphosphanamine

Guidance literature:: With triethylamine; In dichloromethane; for 3h;
DOI:10.1016/j.jorganchem.2008.05.010

Reference yield:

: 1015762-93-2
N-(pyridin-2-ylmethyl)-N-(diphenylphosphanyl)-1,1-diphenylphosphanamine

Guidance literature:: With phosphoric acid; triethylamine; In dichloromethane; water; Inert atmosphere;

Reference yield: 96.0%

: hexacarbonyldiiron(CH₃C(CH₂S)2CH₂OH)

: 1015762-93-2
N-(pyridin-2-ylmethyl)-N-(diphenylphosphanyl)-1,1-diphenylphosphanamine

: 1188444-55-4
[Fe2(CO)4(μ-SCH2)2CMe(CH2OH)((Ph2P)2NCH2(2-C5H4N))]

Guidance literature:: In toluene; (Ar); soln. of complex and ligand was heated for 1.5 h at 110°C under stirring, then cooled to room temp.; solvent was removed under reduced pressure, flash chromy. with silica gel, ethyl acetate-petroleum ether as eluent; elem. anal.;
DOI:10.1039/b903758f