C₁₈H₂₃BrO₇

Base Information

Chemical Name:C₁₈H₂₃BrO₇
CAS No.:951327-36-9
Molecular Formula:C₁₈H₂₃BrO₇
Molecular Weight:431.28
Hs Code.:

C<sub>18</sub>H<sub>23</sub>BrO<sub>7</sub>

Synonyms:C₁₈H₂₃BrO₇

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Chemical Property of C₁₈H₂₃BrO₇

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Technology Process of C₁₈H₂₃BrO₇

There total 4 articles about C₁₈H₂₃BrO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 951327-34-7
C₁₄H₁₅BrO₅

: 107-30-2
chloromethyl methyl ether

: 951327-36-9
C₁₈H₂₃BrO₇

Guidance literature:: With sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 18 ℃; for 3h;
DOI:10.1021/ol071344y

Reference yield:

: C₁₄H₁₃BrO₃

: 951327-36-9
C₁₈H₂₃BrO₇

Guidance literature:: Multi-step reaction with 2 steps

1: 23.3 g / OsO₄; N-methylmorpholine N-oxide / acetone; H₂O; 2-methyl-propan-2-ol / 20 h / 18 °C

2: 91 percent / NaH; i-Pr₂NEt / tetrahydrofuran / 3 h / 0 - 18 °C

With osmium(VIII) oxide; sodium hydride; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; acetone; tert-butyl alcohol;
DOI:10.1021/ol071344y

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 951327-36-9
C₁₈H₂₃BrO₇

Guidance literature:: Multi-step reaction with 3 steps

1: (1S)-(+)-camphor-10-sulfonic acid monohydrate / CH₂Cl₂ / 1 h / -20 °C

2: 23.3 g / OsO₄; N-methylmorpholine N-oxide / acetone; H₂O; 2-methyl-propan-2-ol / 20 h / 18 °C

3: 91 percent / NaH; i-Pr₂NEt / tetrahydrofuran / 3 h / 0 - 18 °C

With osmium(VIII) oxide; (+)-camphor-10-sulfonic acid monohydrate; sodium hydride; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; acetone; tert-butyl alcohol;
DOI:10.1021/ol071344y