(Z)-1-phenyl-4-pentadecen-3-ol

Base Information

Chemical Name:(Z)-1-phenyl-4-pentadecen-3-ol
CAS No.:87837-66-9
Molecular Formula:C₂₁H₃₄O
Molecular Weight:302.5
Hs Code.:

Synonyms:(Z)-1-phenyl-4-pentadecen-3-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-phenyl-4-pentadecen-3-ol

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Technology Process of (Z)-1-phenyl-4-pentadecen-3-ol

There total 4 articles about (Z)-1-phenyl-4-pentadecen-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 147492-41-9
1-phenyl-4-pentadecyn-3-ol

: 87837-66-9
(Z)-1-phenyl-4-pentadecen-3-ol

Guidance literature:: With quinoline; hydrogen; Mn-poisoned Lindlar catalyst; In hexane; for 48h; under 760 Torr; Ambient temperature;
DOI:10.1021/ja00058a059

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 87837-66-9
(Z)-1-phenyl-4-pentadecen-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / cyclopentadienylbis(triphenylphosphine)ruthenium chloride, triethylammonium hexafluorophosphate / dioxane / 8 h / 100 °C

2: 1.) n-butyllithium / 1.) a) ether, hexane, -78 deg C, 15 min, b) 0 deg C, 45 min, 2.) a) ether, hexane, 0 deg C, 30 min, b) RT, 1 h

3: 74 percent / H₂, quinoline / Mn-poisoned Lindlar catalyst / hexane / 48 h / 760 Torr / Ambient temperature

With quinoline; chloro(cyclopentadienyl)bis(triphenylphosphinyl) ruthenium(II); n-butyllithium; hydrogen; triethylammonium hexafluorophosphate; Mn-poisoned Lindlar catalyst; In 1,4-dioxane; hexane;
DOI:10.1021/ja00058a059

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 87837-66-9
(Z)-1-phenyl-4-pentadecen-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) a) ether, hexane, -78 deg C, 15 min, b) 0 deg C, 45 min, 2.) a) ether, hexane, 0 deg C, 30 min, b) RT, 1 h

2: 74 percent / H₂, quinoline / Mn-poisoned Lindlar catalyst / hexane / 48 h / 760 Torr / Ambient temperature

With quinoline; n-butyllithium; hydrogen; Mn-poisoned Lindlar catalyst; In hexane;
DOI:10.1021/ja00058a059