1,2-diamino-3-cyano-4-benzylamino-6-(2,6-dimethylmorpholin-4-yl)quinolinium tosylate

Base Information

Chemical Name:1,2-diamino-3-cyano-4-benzylamino-6-(2,6-dimethylmorpholin-4-yl)quinolinium tosylate
CAS No.:1092536-72-5
Molecular Formula:C₇H₇O₃S*C₂₃H₂₇N₆O
Molecular Weight:574.704
Hs Code.:

Synonyms:1,2-diamino-3-cyano-4-benzylamino-6-(2,6-dimethylmorpholin-4-yl)quinolinium tosylate

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Chemical Property of 1,2-diamino-3-cyano-4-benzylamino-6-(2,6-dimethylmorpholin-4-yl)quinolinium tosylate

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Technology Process of 1,2-diamino-3-cyano-4-benzylamino-6-(2,6-dimethylmorpholin-4-yl)quinolinium tosylate

There total 9 articles about 1,2-diamino-3-cyano-4-benzylamino-6-(2,6-dimethylmorpholin-4-yl)quinolinium tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1092536-70-3
2-amino-3-cyano-4-benzylamino-6-(2,6-dimethylmorpholin-4-yl)quinoline

: 52913-14-1
O-tosylhydroxylamine

: 1092536-72-5
1,2-diamino-3-cyano-4-benzylamino-6-(2,6-dimethylmorpholin-4-yl)quinolinium tosylate

Guidance literature:: In dichloromethane; at 20 ℃; for 5.25h;

Reference yield:

: 141-91-3
2,6-dimethyl morpholine

: 1092536-72-5
1,2-diamino-3-cyano-4-benzylamino-6-(2,6-dimethylmorpholin-4-yl)quinolinium tosylate

Guidance literature:: Multi-step reaction with 7 steps

1.1: 6 h / 120 °C

1.2: pH 6

2.1: cyclohexene / palladium 10% on activated carbon / 6 h / Heating / reflux

3.1: 1,4-dioxane / 4 h / Heating / reflux

3.2: 0.08 h

4.1: sodium hydride / N,N-dimethyl-formamide / 10 h / 20 °C

5.1: trichlorophosphate / 4 h / 120 °C

5.2: 0 °C / pH 8

6.1: 3 h / 125 °C

7.1: dichloromethane / 5.25 h / 20 °C

With sodium hydride; cyclohexene; trichlorophosphate; palladium 10% on activated carbon; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1000018-44-9
2-nitro-5-(2,6-dimethylmorpholin-4-yl)benzoic acid

: 1092536-72-5
1,2-diamino-3-cyano-4-benzylamino-6-(2,6-dimethylmorpholin-4-yl)quinolinium tosylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: cyclohexene / palladium 10% on activated carbon / 6 h / Heating / reflux

2.1: 1,4-dioxane / 4 h / Heating / reflux

2.2: 0.08 h

3.1: sodium hydride / N,N-dimethyl-formamide / 10 h / 20 °C

4.1: trichlorophosphate / 4 h / 120 °C

4.2: 0 °C / pH 8

5.1: 3 h / 125 °C

6.1: dichloromethane / 5.25 h / 20 °C

With sodium hydride; cyclohexene; trichlorophosphate; palladium 10% on activated carbon; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;