1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-trifluoroacetamide-myo-inosite

Base Information

Chemical Name:1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-trifluoroacetamide-myo-inosite
CAS No.:122901-29-5
Molecular Formula:C₄₄H₄₃F₃N₄O₆
Molecular Weight:780.844
Hs Code.:

Synonyms:1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-trifluoroacetamide-myo-inosite

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Chemical Property of 1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-trifluoroacetamide-myo-inosite

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Technology Process of 1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-trifluoroacetamide-myo-inosite

There total 4 articles about 1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-trifluoroacetamide-myo-inosite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 122901-25-1
1L-1,4,5,6-tetra-O-benzyl-4-C-benzyloxymethyl-2-desoxy-2-trifluoroacetamido-3-O-<(trifluoromethyl)sulfonyl>-muco-inosite

: 122901-29-5
1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-trifluoroacetamide-myo-inosite

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; for 3h; Ambient temperature;

Reference yield:

: 106989-01-9
1L-2-azido-1,4,5,6-tetra-O-benzyl-2-desoxy-4-C-(benzyloxymethyl)-muco-inosit

: 122901-29-5
1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-trifluoroacetamide-myo-inosite

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / NaBH₄ / 4 percent NiCl₂ / ethanol

2: 64 percent / methanol / 65 h / Ambient temperature

3: 98 percent / pyridine / CH₂Cl₂ / 0.5 h / -40 °C

4: 89 percent / NaN₃ / dimethylformamide / 3 h / Ambient temperature

With pyridine; sodium tetrahydroborate; sodium azide; nickel dichloride; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 122901-18-2
1L-2-amino-1,4,5,6-tetra-O-benzyl-4-C-bezyloxymethyl-2-desoxy-muco-inosite

: 122901-29-5
1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-trifluoroacetamide-myo-inosite

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / methanol / 65 h / Ambient temperature

2: 98 percent / pyridine / CH₂Cl₂ / 0.5 h / -40 °C

3: 89 percent / NaN₃ / dimethylformamide / 3 h / Ambient temperature

With pyridine; sodium azide; In methanol; dichloromethane; N,N-dimethyl-formamide;