5,5',5''-((phenylsilanetriyl)tris(benzene-4,1-diyl))tris(2-phenyl-1,3,4-oxadiazole)

Base Information

Chemical Name:5,5',5''-((phenylsilanetriyl)tris(benzene-4,1-diyl))tris(2-phenyl-1,3,4-oxadiazole)
CAS No.:1361962-07-3
Molecular Formula:C₄₈H₃₂N₆O₃Si
Molecular Weight:768.906
Hs Code.:

Synonyms:5,5',5''-((phenylsilanetriyl)tris(benzene-4,1-diyl))tris(2-phenyl-1,3,4-oxadiazole)

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Chemical Property of 5,5',5''-((phenylsilanetriyl)tris(benzene-4,1-diyl))tris(2-phenyl-1,3,4-oxadiazole)

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Technology Process of 5,5',5''-((phenylsilanetriyl)tris(benzene-4,1-diyl))tris(2-phenyl-1,3,4-oxadiazole)

There total 3 articles about 5,5',5''-((phenylsilanetriyl)tris(benzene-4,1-diyl))tris(2-phenyl-1,3,4-oxadiazole) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 18039-42-4,3999-10-8
5-Phenyl-1H-tetrazole

: 445429-82-3
4,4',4''-(phenylsilanetriyl)tribenzoyl chloride

: 1361962-07-3
5,5',5''-((phenylsilanetriyl)tris(benzene-4,1-diyl))tris(2-phenyl-1,3,4-oxadiazole)

Guidance literature:: With pyridine; at 95 ℃; for 24h;
DOI:10.1021/ol301734a

Reference yield:

: 18870-40-1
phenyltri-p-tolylsilane

: 1361962-07-3
5,5',5''-((phenylsilanetriyl)tris(benzene-4,1-diyl))tris(2-phenyl-1,3,4-oxadiazole)

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; potassium permanganate / water / 16 h / 20 - 95 °C

2: oxalyl dichloride / N,N-dimethyl-formamide; toluene / 12 h / 80 °C

3: pyridine / 24 h / 95 °C

With pyridine; potassium permanganate; oxalyl dichloride; In water; N,N-dimethyl-formamide; toluene; 3: |Huisgen Tetrazole Rearrangement;
DOI:10.1021/ol301734a

Reference yield:

: 61414-17-3
4,4′,4″-(phenylsilanetriyl)tribenzoic acid

: 1361962-07-3
5,5',5''-((phenylsilanetriyl)tris(benzene-4,1-diyl))tris(2-phenyl-1,3,4-oxadiazole)

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / N,N-dimethyl-formamide; toluene / 12 h / 80 °C

2: pyridine / 24 h / 95 °C

With pyridine; oxalyl dichloride; In N,N-dimethyl-formamide; toluene; 2: |Huisgen Tetrazole Rearrangement;
DOI:10.1021/ol301734a