N-cyano-N'-<5-cyano-2-(1,1-dimethylethyl)phenyl>carbamimidic acid phenyl ester

Base Information

Chemical Name:N-cyano-N'-<5-cyano-2-(1,1-dimethylethyl)phenyl>carbamimidic acid phenyl ester
CAS No.:166263-22-5
Molecular Formula:C₁₉H₁₈N₄O
Molecular Weight:318.378
Hs Code.:

Synonyms:N-cyano-N'-<5-cyano-2-(1,1-dimethylethyl)phenyl>carbamimidic acid phenyl ester

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Chemical Property of N-cyano-N'-<5-cyano-2-(1,1-dimethylethyl)phenyl>carbamimidic acid phenyl ester

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Technology Process of N-cyano-N'-<5-cyano-2-(1,1-dimethylethyl)phenyl>carbamimidic acid phenyl ester

There total 4 articles about N-cyano-N'-<5-cyano-2-(1,1-dimethylethyl)phenyl>carbamimidic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 253185-03-4,253185-04-5
tert-butylbenzene

: 166263-22-5
N-cyano-N'-<5-cyano-2-(1,1-dimethylethyl)phenyl>carbamimidic acid phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / HNO₃, H₂SO₄

2: 86 percent / aq. sodium sulfide, sulfur

3: 1.) conc. HCl, aq. NaNO₂, 2.) aq. KCN / 1.) EtOH, 0 deg C, 10 min, 2.) EtOH, 100 deg C, 15 min

4: SnCl₂*2H₂O / ethanol / 0.75 h / Heating

5: 1.) NaH / 1.) THF, RT, 15 min, 2.) THF, reflux, 4 h

With hydrogenchloride; potassium cyanide; sodium sulfide; sulfuric acid; nitric acid; sodium hydride; sulfur; tin(ll) chloride; sodium nitrite; In ethanol;
DOI:10.1021/jm950646f

Reference yield:

: 31951-12-9
4-tert-butyl-3-nitro-phenylamine

: 166263-22-5
N-cyano-N'-<5-cyano-2-(1,1-dimethylethyl)phenyl>carbamimidic acid phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) conc. HCl, aq. NaNO₂, 2.) aq. KCN / 1.) EtOH, 0 deg C, 10 min, 2.) EtOH, 100 deg C, 15 min

2: SnCl₂*2H₂O / ethanol / 0.75 h / Heating

3: 1.) NaH / 1.) THF, RT, 15 min, 2.) THF, reflux, 4 h

With hydrogenchloride; potassium cyanide; sodium hydride; tin(ll) chloride; sodium nitrite; In ethanol;
DOI:10.1021/jm950646f

Reference yield:

: 70634-25-2
4-(1,1-Dimethylethyl)-3-nitro-benzonitrile

: 166263-22-5
N-cyano-N'-<5-cyano-2-(1,1-dimethylethyl)phenyl>carbamimidic acid phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SnCl₂*2H₂O / ethanol / 0.75 h / Heating

2: 1.) NaH / 1.) THF, RT, 15 min, 2.) THF, reflux, 4 h

With sodium hydride; tin(ll) chloride; In ethanol;
DOI:10.1021/jm950646f