8-benzoyl-2,2-dimethyl-1,4,8-triazaspiro<4.5>decane

Base Information

Chemical Name:8-benzoyl-2,2-dimethyl-1,4,8-triazaspiro<4.5>decane
CAS No.:80028-50-8
Molecular Formula:C₁₆H₂₃N₃O
Molecular Weight:273.378
Hs Code.:

Synonyms:8-benzoyl-2,2-dimethyl-1,4,8-triazaspiro<4.5>decane

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Chemical Property of 8-benzoyl-2,2-dimethyl-1,4,8-triazaspiro<4.5>decane

Chemical Property:

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Technology Process of 8-benzoyl-2,2-dimethyl-1,4,8-triazaspiro<4.5>decane

There total 1 articles about 8-benzoyl-2,2-dimethyl-1,4,8-triazaspiro<4.5>decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24686-78-0
1-Benzoyl-4-piperidone

: 811-93-8
1,1-dimethylethylenediamine

: 80028-50-8
8-benzoyl-2,2-dimethyl-1,4,8-triazaspiro<4.5>decane

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 14h; Heating;
DOI:10.1021/ja00367a029

Reference yield: 64.0%

: 80028-50-8
8-benzoyl-2,2-dimethyl-1,4,8-triazaspiro<4.5>decane

: 2258-42-6
formyl acetic anhydride

: 80028-53-1
8-benzoyl-2,2-dimethyl-4-formyl-1,4,8-triazaspiro<4.5>decane

Guidance literature:: In diethyl ether; dichloromethane; at 25 ℃; for 13h;
DOI:10.1021/ja00367a029

Reference yield:

: 80028-50-8
8-benzoyl-2,2-dimethyl-1,4,8-triazaspiro<4.5>decane

: 80028-54-2
8-benzoyl-2,2-dimethyl-4-formyl-1,4,8-triazaspiro<4.5>decanyl-1-oxy

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / diethyl ether; CH₂Cl₂ / 13 h / 25 °C

2: 68 percent / 85percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 25 °C

With 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1021/ja00367a029