dimethyl(thexyl)silyl 6-O-benzyl-2-deoxy-2-(dimethylmaleimido)-3-O-levulinoyl-β-D-glucopyranoside

Base Information

• Chemical Name: dimethyl(thexyl)silyl 6-O-benzyl-2-deoxy-2-(dimethylmaleimido)-3-O-levulinoyl-β-D-glucopyranoside
• CAS No.: 1010440-55-7
• Molecular Formula: C₃₂H₄₇NO₉Si
• Molecular Weight: 617.812

Synonyms:dimethyl(thexyl)silyl 6-O-benzyl-2-deoxy-2-(dimethylmaleimido)-3-O-levulinoyl-β-D-glucopyranoside

Chemical Property of dimethyl(thexyl)silyl 6-O-benzyl-2-deoxy-2-(dimethylmaleimido)-3-O-levulinoyl-β-D-glucopyranoside

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Technology Process of dimethyl(thexyl)silyl 6-O-benzyl-2-deoxy-2-(dimethylmaleimido)-3-O-levulinoyl-β-D-glucopyranoside

There total 1 articles about dimethyl(thexyl)silyl 6-O-benzyl-2-deoxy-2-(dimethylmaleimido)-3-O-levulinoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

dimethyl(thexyl)silyl 4,6-O-benzylidene-2-deoxy-2-(dimethylmaleimido)-3-O-levulinoyl-β-D-glucopyranoside (1010440-54-6) → dimethyl(thexyl)silyl 6-O-benzyl-2-deoxy-2-(dimethylmaleimido)-3-O-levulinoyl-β-D-glucopyranoside (1010440-55-7)

Guidance literature:

With triethylsilane; trifluoroacetic acid; trifluoroacetic anhydride; In dichloromethane; at 0 ℃; for 4h;

DOI:10.1002/ejoc.200700698

Reference yield: 68.0%

O-2,6-di-O-acetyl-3,4-di-O-benzyl-α-D-glucopyranosyl trichloroacetimidate (1010440-34-2) + dimethyl(thexyl)silyl 6-O-benzyl-2-deoxy-2-(dimethylmaleimido)-3-O-levulinoyl-β-D-glucopyranoside (1010440-55-7) → dimethyl(thexyl)silyl 2,6-di-O-acetyl-3,4-di-O-benzyl-β-D-glucopyranosyl-(1->4)-6-O-benzyl-2-deoxy-2-(dimethylmaleimido)-3-O-levulinoyl-β-D-glucopyranoside (1010440-56-8)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 1.5h;

DOI:10.1002/ejoc.200700698

upstream raw materials:

dimethyl(thexyl)silyl 4,6-O-benzylidene-2-deoxy-2-(dimethylmaleimido)-3-O-levulinoyl-β-D-glucopyranoside

Downstream raw materials:

dimethyl(thexyl)silyl 2,6-di-O-acetyl-3,4-di-O-benzyl-β-D-glucopyranosyl-(1->4)-6-O-benzyl-2-deoxy-2-(dimethylmaleimido)-3-O-levulinoyl-β-D-glucopyranoside

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