6-O-(2-Amino-2-deoxy-α-D-galactopyranosyl)-3-O-dibenzylphosphoryl-D-chiro-inositol

Base Information

Chemical Name:6-O-(2-Amino-2-deoxy-α-D-galactopyranosyl)-3-O-dibenzylphosphoryl-D-chiro-inositol
CAS No.:132891-83-9
Molecular Formula:C₁₂H₂₄NO₁₃P
Molecular Weight:421.295
Hs Code.:

Synonyms:6-O-(2-Amino-2-deoxy-α-D-galactopyranosyl)-3-O-dibenzylphosphoryl-D-chiro-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-O-(2-Amino-2-deoxy-α-D-galactopyranosyl)-3-O-dibenzylphosphoryl-D-chiro-inositol

Chemical Property:

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Technology Process of 6-O-(2-Amino-2-deoxy-α-D-galactopyranosyl)-3-O-dibenzylphosphoryl-D-chiro-inositol

There total 31 articles about 6-O-(2-Amino-2-deoxy-α-D-galactopyranosyl)-3-O-dibenzylphosphoryl-D-chiro-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₂₄H₄₀NO₁₃P

: 132891-83-9
6-O-(2-Amino-2-deoxy-α-D-galactopyranosyl)-3-O-dibenzylphosphoryl-D-chiro-inositol

Guidance literature:: With acetic acid; at 80 ℃; for 2.5h;
DOI:10.1016/0040-4020(91)80003-K

Reference yield: 73.0%

: 6-O-(2-Azido-2-deoxy-α-D-glucopyranosyl)-1,2;4,5-di-O-cyclopropylidene-3-O-dibenzylphosphoryl-D-myo-inositol

: 132891-83-9
4-O-(2-Amino-2-deoxy-α-D-glucopyranosyl)-1-O-dihydrogenphosphoryl-D-myo-inositol

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; water; at 25 ℃; for 24h;
DOI:10.1016/0040-4020(91)80003-K

Reference yield:

: 34361-60-9,55123-24-5,55123-26-7,62012-78-6,104873-71-4
1,2:4,5-dicyclohexylidene-myo-inositol

: 132891-83-9
6-O-(2-Amino-2-deoxy-α-D-galactopyranosyl)-3-O-dibenzylphosphoryl-D-chiro-inositol

Guidance literature:: Multi-step reaction with 11 steps

1: 75 percent / pyridine / CH₂Cl₂ / 2 h / -40 °C

2: 36 percent / Et₃N, DMAP / CH₂Cl₂ / 25 °C

3: tetrabutylammonium nitrate / dimethylformamide / 16 h / 100 °C

4: hydrogen / 10 percent Pd-C / methanol / 2.5 h / 25 °C / 2844.3 Torr

5: tetrazole / CH₂Cl₂ / 25 °C

6: m-chlorperbenzoic acid / CH₂Cl₂ / 0 °C

7: NH₃ / methanol / 36 h / 25 °C

8: 57 percent / silver triflate, tetramethylurea, molecular sieves 4 Angstroem / CH₂Cl₂ / 24 h / 25 °C

9: 75 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.5 h / 25 °C

10: 90 percent / hydrogen / 10 percent Pd-C / methanol; H₂O / 18 h / 25 °C

11: 86 percent / aq. acetic acid / 2.5 h / 80 °C

With pyridine; 1H-tetrazole; dmap; 4 A molecular sieve; tetrabutyl ammonium fluoride; ammonia; hydrogen; silver trifluoromethanesulfonate; tetrabutylammonium nitrate; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; tetramethylurea; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(91)80003-K