2-(2,4-difluorophenyl)-4-(2,4,6-trimethylphenyl)pyridine

Base Information

Chemical Name:2-(2,4-difluorophenyl)-4-(2,4,6-trimethylphenyl)pyridine
CAS No.:1435909-79-7
Molecular Formula:C₂₀H₁₇F₂N
Molecular Weight:309.358
Hs Code.:

Synonyms:2-(2,4-difluorophenyl)-4-(2,4,6-trimethylphenyl)pyridine

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Chemical Property of 2-(2,4-difluorophenyl)-4-(2,4,6-trimethylphenyl)pyridine

Chemical Property:

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Technology Process of 2-(2,4-difluorophenyl)-4-(2,4,6-trimethylphenyl)pyridine

There total 3 articles about 2-(2,4-difluorophenyl)-4-(2,4,6-trimethylphenyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153034-86-7
2-chloro-4-iodopyridine

: 1435909-79-7
2-(2,4-difluorophenyl)-4-(2,4,6-trimethylphenyl)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 72 h / 95 °C / Inert atmosphere

2: triphenylphosphine; sodium carbonate; palladium diacetate / water; 1,2-dimethoxyethane / 24 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; sodium carbonate; potassium carbonate; triphenylphosphine; In 1,4-dioxane; 1,2-dimethoxyethane; water;
DOI:10.1021/cm4010773

Reference yield:

: 5980-97-2
mesitylboronic acid

: 1435909-79-7
2-(2,4-difluorophenyl)-4-(2,4,6-trimethylphenyl)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 72 h / 95 °C / Inert atmosphere

2: triphenylphosphine; sodium carbonate; palladium diacetate / water; 1,2-dimethoxyethane / 24 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; sodium carbonate; potassium carbonate; triphenylphosphine; In 1,4-dioxane; 1,2-dimethoxyethane; water;
DOI:10.1021/cm4010773

Reference yield:

: 73583-37-6
2-chloro-4-bromopyridine

: 5980-97-2
mesitylboronic acid

: 1435909-79-7
2-(2,4-difluorophenyl)-4-(2,4,6-trimethylphenyl)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 24 h / 95 °C / Darkness; Inert atmosphere

2: tetrabutylammomium bromide; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 24 h / 95 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate; In toluene;