methyl 2-(4-amino-2,5-dimethylbenzyl)-4-(4-chlorophenyl)-1,3-thiazole-5-carboxylate

Base Information

Chemical Name:methyl 2-(4-amino-2,5-dimethylbenzyl)-4-(4-chlorophenyl)-1,3-thiazole-5-carboxylate
CAS No.:1421922-19-1
Molecular Formula:C₂₀H₁₉ClN₂O₂S
Molecular Weight:386.902
Hs Code.:

Synonyms:methyl 2-(4-amino-2,5-dimethylbenzyl)-4-(4-chlorophenyl)-1,3-thiazole-5-carboxylate

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Chemical Property of methyl 2-(4-amino-2,5-dimethylbenzyl)-4-(4-chlorophenyl)-1,3-thiazole-5-carboxylate

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Technology Process of methyl 2-(4-amino-2,5-dimethylbenzyl)-4-(4-chlorophenyl)-1,3-thiazole-5-carboxylate

There total 6 articles about methyl 2-(4-amino-2,5-dimethylbenzyl)-4-(4-chlorophenyl)-1,3-thiazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421922-18-0
methyl 4-(4-chlorophenyl)-2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazole-5-carboxylate

: 1421922-19-1
methyl 2-(4-amino-2,5-dimethylbenzyl)-4-(4-chlorophenyl)-1,3-thiazole-5-carboxylate

Guidance literature:: With water; iron; ammonium chloride; In ethanol; for 2h; Reflux;

Reference yield:

: 16213-85-7
(2,5-dimethylphenyl)acetonitrile

: 1421922-19-1
methyl 2-(4-amino-2,5-dimethylbenzyl)-4-(4-chlorophenyl)-1,3-thiazole-5-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: nitric acid / 0.5 h / Cooling with ice

2: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

3: isopropyl alcohol / 2 h / 80 °C

4: ammonium chloride; iron; water / ethanol / 2 h / Reflux

With hydrogenchloride; water; nitric acid; iron; ammonium chloride; O,O-Diethyl hydrogen phosphorodithioate; In ethanol; ethyl acetate; isopropyl alcohol;

Reference yield:

: 1421922-03-3
(2,5-dimethyl-4-nitrophenyl)acetonitrile

: 1421922-19-1
methyl 2-(4-amino-2,5-dimethylbenzyl)-4-(4-chlorophenyl)-1,3-thiazole-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

2: isopropyl alcohol / 2 h / 80 °C

3: ammonium chloride; iron; water / ethanol / 2 h / Reflux

With hydrogenchloride; water; iron; ammonium chloride; O,O-Diethyl hydrogen phosphorodithioate; In ethanol; ethyl acetate; isopropyl alcohol;