(Z)-N-((E)-3-(iodo(phenyl)methylene)isobenzofuran-1(3H)-ylidene)methanamine

Base Information

Chemical Name:(Z)-N-((E)-3-(iodo(phenyl)methylene)isobenzofuran-1(3H)-ylidene)methanamine
CAS No.:1408314-36-2
Molecular Formula:C₁₆H₁₂INO
Molecular Weight:361.182
Hs Code.:

Synonyms:(Z)-N-((E)-3-(iodo(phenyl)methylene)isobenzofuran-1(3H)-ylidene)methanamine

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Chemical Property of (Z)-N-((E)-3-(iodo(phenyl)methylene)isobenzofuran-1(3H)-ylidene)methanamine

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Technology Process of (Z)-N-((E)-3-(iodo(phenyl)methylene)isobenzofuran-1(3H)-ylidene)methanamine

There total 4 articles about (Z)-N-((E)-3-(iodo(phenyl)methylene)isobenzofuran-1(3H)-ylidene)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 110166-72-8
2-(2'-phenylethynyl)-N-methyl benzamide

: 1408314-36-2
(Z)-N-((E)-3-(iodo(phenyl)methylene)isobenzofuran-1(3H)-ylidene)methanamine

Guidance literature:: With lithium perchlorate; sodium iodide; In acetonitrile; at 20 ℃; for 5h; regioselective reaction; Electrochemical reaction;
DOI:10.1039/d1ob00953b

Reference yield: 72.0%

: 110166-72-8
2-(2'-phenylethynyl)-N-methyl benzamide

: 1408314-36-2
(Z)-N-((E)-3-(iodo(phenyl)methylene)isobenzofuran-1(3H)-ylidene)methanamine

: 1408314-39-5
(1Z)-4-iodo-N-methyl-3-phenyl-1H-isochromen-1-imine

Guidance literature:: With iodine; sodium hydrogencarbonate; In acetonitrile; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1021/jo3017378

Reference yield:

: 58084-22-3
2-iodo-N-methyl-benzamide

: 1408314-36-2
(Z)-N-((E)-3-(iodo(phenyl)methylene)isobenzofuran-1(3H)-ylidene)methanamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 1,2-dichloro-ethane / 0.33 h / 20 °C / Inert atmosphere

1.2: 4 h / 70 °C / Inert atmosphere

2.1: lithium perchlorate; sodium iodide / acetonitrile / 5 h / 20 °C / Electrochemical reaction

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium perchlorate; triethylamine; sodium iodide; In 1,2-dichloro-ethane; acetonitrile;
DOI:10.1039/d1ob00953b